Naderi-Samani Hamed, Shoja Razavi Reza, Loghman-Estarki Mohammad Reza, Ramazani Mazaher
Department of Materials Engineering, Malek Ashtar University of Technology, P.O. Box 83145/115, Shahin Shahr, Iran.
Department of Materials Engineering, Malek Ashtar University of Technology, P.O. Box 83145/115, Shahin Shahr, Iran.
Ultrason Sonochem. 2017 Sep;38:306-316. doi: 10.1016/j.ultsonch.2017.03.009. Epub 2017 Mar 14.
In this research, solvent based polyamide - imide (PAI)/clay nanocomposites were prepared successfully using the solution dispersion technique. With the assistance of the ultrasonic wave, the effect of the ultrasonic wave time on the microstructure of 3wt% PAI/C20A nanocomposite (NC) was investigated. Then, the best ultrasonic parameters were selected and the effects of the concentration of Cloisite 20A (C20A) (1, 3 and 5wt% C20A) on the microstructure and mechanical properties (adhesion, hardness, flexibility, wear and impact) of NCs were investigated. The PAI, C20A and nanocomposites (NC)s were characterized by Fourier transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FE-SEM), energy dispersive X-ray analysis (EDX), and Wide-angle X-ray diffraction (WAXD). The results showed that the sample with 1 and 3wt% C20A had better mechanical properties, as compared to the pure PAI and the 5wt% NC.
在本研究中,采用溶液分散技术成功制备了溶剂型聚酰胺 - 酰亚胺(PAI)/粘土纳米复合材料。在超声波的辅助下,研究了超声时间对3wt% PAI/C20A纳米复合材料(NC)微观结构的影响。然后,选择了最佳超声参数,并研究了Cloisite 20A(C20A)浓度(1、3和5wt% C20A)对纳米复合材料微观结构和力学性能(附着力、硬度、柔韧性、耐磨性和冲击性)的影响。通过傅里叶变换红外光谱(FTIR)、场发射扫描电子显微镜(FE-SEM)、能量色散X射线分析(EDX)和广角X射线衍射(WAXD)对PAI、C20A和纳米复合材料(NC)进行了表征。结果表明,与纯PAI和5wt% NC相比,含有1wt%和3wt% C20A的样品具有更好的力学性能。