Patidar Rajesh, Rebary Babulal, Sanghani Dhruti A, Bhadu Gopala Ram, Paul Parimal
Analytical Division & Centralized Instrument facility, CSIR-Central Salt & Marine Chemicals Research institute, Bhavnagar, Gujarat, India.
P.D. Patel Institute of Applied Sciences, Charotar University of Science & Technology, Changa, Anand, Gujarat, India.
Luminescence. 2017 Dec;32(8):1466-1472. doi: 10.1002/bio.3346. Epub 2017 Jun 21.
Two green methods (microwave and hydrothermal) were employed for the preparation of water dispersible fluorescent carbon nanoparticles (CNPs) from activated charcoal. Microwave and hydrothermally synthesized carbon nanoparticles, (MW-CNPs) and (HT-CNPs), respectively were characterized by microscopic and spectroscopic techniques. A detailed study of their fluorescence characteristics was made. MW-CNPs and HT-CNPs were tested for metal ion selectivity in aqueous medium. MW-CNPs showed selectivity for Fe among the tested metal ions and important studies such as for interference, linear range and limit of detection were carried out. The application of MW-CNPs for detection of Fe in water was demonstrated.
采用两种绿色方法(微波法和水热法)从活性炭制备水分散性荧光碳纳米颗粒(CNPs)。分别通过显微镜和光谱技术对微波合成的碳纳米颗粒(MW-CNPs)和水热合成的碳纳米颗粒(HT-CNPs)进行了表征。对它们的荧光特性进行了详细研究。测试了MW-CNPs和HT-CNPs在水介质中的金属离子选择性。MW-CNPs在测试的金属离子中对Fe表现出选择性,并开展了诸如干扰、线性范围和检测限等重要研究。证明了MW-CNPs在水中检测Fe的应用。