Laundy David, Sawhney Kawal, Dhamgaye Vishal
Diamond Light Source, Harwell Science and Innovation Campus, Didcot, Oxon OX11 0DE, UK.
Indus Synchrotrons Utilisation Division, Raja Ramanna Centre for Advanced Technology, Indore 452012, India.
J Synchrotron Radiat. 2017 Jul 1;24(Pt 4):744-749. doi: 10.1107/S1600577517006038. Epub 2017 May 30.
X-ray mirrors are widely used at synchrotron radiation sources for focusing X-rays into focal spots of size less than 1 µm. The ability of the beamline optics to change the size of this spot over a range up to tens of micrometres can be an advantage for many experiments such as X-ray microprobe and X-ray diffraction from micrometre-scale crystals. It is a requirement that the beam size change should be reproducible and it is often essential that the change should be rapid, for example taking less than 1 s, in order to allow high data collection rates at modern X-ray sources. In order to provide a controlled broadening of the focused spot of an X-ray mirror, a series of refractive optical elements have been fabricated and installed immediately before the mirror. By translation, a new refractive element is moved into the X-ray beam allowing a variation in the size of the focal spot in the focusing direction. Measurements using a set of prefabricated refractive structures with a test mirror showed that the focused beam size could be varied from less than 1 µm to over 10 µm for X-rays in the energy range 10-20 keV. As the optics is in-line with the X-ray beam, there is no effect on the centroid position of the focus. Accurate positioning of the refractive optics ensures reproducibility in the focused beam profile and no additional re-alignment of the optics is required.
X射线镜在同步辐射源中被广泛应用,用于将X射线聚焦成尺寸小于1微米的焦点。对于许多实验,如X射线微探针和微米级晶体的X射线衍射,光束线光学元件在高达几十微米的范围内改变该光斑尺寸的能力可能是一个优势。要求光束尺寸的变化应具有可重复性,并且通常至关重要的是变化应迅速,例如小于1秒,以便在现代X射线源处实现高数据采集率。为了对X射线镜的聚焦光斑进行可控展宽,已制造了一系列折射光学元件,并将其紧挨着镜子安装。通过平移,一个新的折射元件移入X射线束,从而使聚焦光斑在聚焦方向上的尺寸发生变化。使用一组预制折射结构和一个测试镜进行的测量表明,对于能量范围为10 - 20千电子伏的X射线,聚焦光束尺寸可从小于1微米变化到超过10微米。由于光学元件与X射线束共线,因此对焦点的质心位置没有影响。折射光学元件的精确定位确保了聚焦光束轮廓的可重复性,并且无需对光学元件进行额外的重新对准。