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在具有原位压力测定功能的金刚石对顶砧高压腔室中对氩气压力介质进行低温加载。

Cryogenic loading of argon pressure medium in diamond anvil high pressure cells with in situ pressure determination.

作者信息

Pugh E

机构信息

School of Physical Sciences, University of Kent, Canterbury, Kent CT2 7NH, United Kingdom.

出版信息

Rev Sci Instrum. 2017 Jun;88(6):065115. doi: 10.1063/1.4989699.

Abstract

A versatile system for cryogenic loading of argon pressure medium into the sample space of a diamond anvil cell has been developed. The system has been designed such that, with suitable adaptors, a wide range of diamond anvil cell designs can be pressurized. The pressure in the cell can be monitored during pressurization using the ruby fluorescence method via optical fiber access into the loading chamber. This enables the precise and accurate setting of the loading pressure in the cell.

摘要

已开发出一种通用系统,用于将氩气压力介质低温加载到金刚石对顶砧室的样品空间中。该系统的设计使得通过合适的适配器,可以对多种金刚石对顶砧室设计进行加压。在加压过程中,可以通过光纤进入加载室,使用红宝石荧光法监测室中的压力。这使得能够精确且准确地设定室中的加载压力。

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