Katogi Hideaki, Takemura Kenichi, Akiyama Motoki
Department of Mechanical Engineering, Kanagawa University, 3-27-1 Rokkakubashi, Kanagawa-ku, Yokohama, Kanagawa 221-8686, Japan.
Materials (Basel). 2016 Jul 14;9(7):573. doi: 10.3390/ma9070573.
This study investigated the residual tensile properties of plain woven jute fiber reinforced poly(lactic acid) (PLA) during thermal cycling. Temperature ranges of thermal cycling tests were 35-45 °C and 35-55 °C. The maximum number of cycles was 10³ cycles. The quasi-static tensile tests of jute fiber, PLA, and composite were conducted after thermal cycling tests. Thermal mechanical analyses of jute fiber and PLA were conducted after thermal cycling tests. Results led to the following conclusions. For temperatures of 35-45 °C, tensile strength of composite at 10³ cycles decreased 10% compared to that of composite at 0 cycles. For temperatures of 35-55 °C, tensile strength and Young's modulus of composite at 10³ cycles decreased 15% and 10%, respectively, compared to that of composite at 0 cycles. Tensile properties and the coefficient of linear expansion of PLA and jute fiber remained almost unchanged after thermal cycling tests. From observation of a fracture surface, the length of fiber pull out in the fracture surface of composite at 10³ cycles was longer than that of composite at 0 cycles. Therefore, tensile properties of the composite during thermal cycling were decreased, probably because of the decrease of interfacial adhesion between the fiber and resin.
本研究调查了平纹黄麻纤维增强聚乳酸(PLA)在热循环过程中的残余拉伸性能。热循环试验的温度范围为35 - 45°C和35 - 55°C。最大循环次数为10³次循环。在热循环试验后进行了黄麻纤维、PLA和复合材料的准静态拉伸试验。在热循环试验后对黄麻纤维和PLA进行了热机械分析。结果得出以下结论。对于35 - 45°C的温度,复合材料在10³次循环时的拉伸强度比0次循环时的复合材料降低了10%。对于35 - 55°C的温度,复合材料在10³次循环时的拉伸强度和杨氏模量分别比0次循环时的复合材料降低了15%和10%。热循环试验后,PLA和黄麻纤维的拉伸性能及线性膨胀系数几乎保持不变。从断口表面观察,复合材料在10³次循环时断口表面的纤维拔出长度比0次循环时的复合材料更长。因此,复合材料在热循环过程中的拉伸性能下降,可能是由于纤维与树脂之间界面粘结力的降低。