Pyka Grzegorz, Kerckhofs Greet, Papantoniou Ioannis, Speirs Mathew, Schrooten Jan, Wevers Martine
Department of Metallurgy and Materials Engineering, KU Leuven, Kasteelpark Arenberg 44 PB2450, Leuven B-3001, Belgium.
Prometheus, Division of Skeletal Tissue Engineering, KU Leuven, O&N 1, Herestraat 49 PB813, Leuven B-3000, Belgium.
Materials (Basel). 2013 Oct 22;6(10):4737-4757. doi: 10.3390/ma6104737.
Additive manufacturing (AM) is a production method that enables the building of porous structures with a controlled geometry. However, there is a limited control over the final surface of the product. Hence, complementary surface engineering strategies are needed. In this work, design of experiments (DoE) was used to customize post AM surface treatment for 3D selective laser melted Ti6Al4V open porous structures for bone tissue engineering. A two-level three-factor full factorial design was employed to assess the individual and interactive effects of the surface treatment duration and the concentration of the chemical etching solution on the final surface roughness and beam thickness of the treated porous structures. It was observed that the concentration of the surface treatment solution was the most important factor influencing roughness reduction. The designed beam thickness decreased the effectiveness of the surface treatment. In this case study, the optimized processing conditions for AM production and the post-AM surface treatment were defined based on the DoE output and were validated experimentally. This allowed the production of customized 3D porous structures with controlled surface roughness and overall morphological properties, which can assist in more controlled evaluation of the effect of surface roughness on various functional properties.
增材制造(AM)是一种能够构建具有可控几何形状的多孔结构的生产方法。然而,对产品的最终表面控制有限。因此,需要互补的表面工程策略。在这项工作中,实验设计(DoE)被用于为用于骨组织工程的3D选择性激光熔化Ti6Al4V开放多孔结构定制增材制造后的表面处理。采用两级三因素全因子设计来评估表面处理持续时间和化学蚀刻溶液浓度对处理后的多孔结构的最终表面粗糙度和梁厚度的单独和交互作用。观察到表面处理溶液的浓度是影响粗糙度降低的最重要因素。设计的梁厚度降低了表面处理的效果。在这个案例研究中,基于实验设计的输出定义了增材制造生产和增材制造后表面处理的优化工艺条件,并通过实验进行了验证。这使得能够生产具有可控表面粗糙度和整体形态特性的定制3D多孔结构,这有助于更可控地评估表面粗糙度对各种功能特性的影响。