Voronov D L, Gullikson E M, Padmore H A
Opt Express. 2017 Sep 18;25(19):23334-23342. doi: 10.1364/OE.25.023334.
A process for fabrication of ultra-precise diffraction gratings for high resolution x-ray spectroscopy was developed. A grating pattern with constant or variable line spacing (VLS) is recorded on a quartz plate by use of e-beam lithography with nanometer scale accuracy of the groove placement. The pattern is transferred to a massive grating blank by large area nanoimprint followed by dry or/and wet etching for groove shaping. High fidelity of the nanoimprint transfer step was confirmed by differential wavefront measurements. Successful implementation of the suggested fabrication approach was demonstrated by fabrication of a lamellar 900 lines/mm VLS grating for a soft x-ray fluorescence spectrometer.
开发了一种用于高分辨率X射线光谱学的超精密衍射光栅制造工艺。通过使用具有纳米级刻槽放置精度的电子束光刻技术,在石英板上记录具有恒定或可变线间距(VLS)的光栅图案。通过大面积纳米压印将图案转移到块状光栅坯料上,然后进行干法或/和湿法蚀刻以形成刻槽形状。通过差分波前测量证实了纳米压印转移步骤的高保真度。通过为软X射线荧光光谱仪制造层状900线/毫米VLS光栅,证明了所建议制造方法的成功实施。