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从纳米颗粒的透射电子显微镜图像测量表面应变的准确性。

Accuracy of surface strain measurements from transmission electron microscopy images of nanoparticles.

作者信息

Madsen Jacob, Liu Pei, Wagner Jakob B, Hansen Thomas W, Schiøz Jakob

机构信息

Department of Physics, Technical University of Denmark, Fysikvej, Building 311, 2800 Kongens Lyngby, Denmark.

Center for Electron Nanoscopy, Technical University of Denmark, Fysikvej, Building 311, 2800 Kongens Lyngby, Denmark.

出版信息

Adv Struct Chem Imaging. 2017;3(1):14. doi: 10.1186/s40679-017-0047-0. Epub 2017 Oct 25.

Abstract

Strain analysis from high-resolution transmission electron microscopy (HRTEM) images offers a convenient tool for measuring strain in materials at the atomic scale. In this paper we present a theoretical study of the precision and accuracy of surface strain measurements directly from aberration-corrected HRTEM images. We examine the influence of defocus, crystal tilt and noise, and find that absolute errors of at least 1-2% strain should be expected. The model structures include surface relaxations determined using molecular dynamics, and we show that this is important for correctly evaluating the errors introduced by image aberrations.

摘要

高分辨率透射电子显微镜(HRTEM)图像的应变分析为在原子尺度上测量材料应变提供了一种便捷工具。在本文中,我们对直接从像差校正的HRTEM图像进行表面应变测量的精度和准确性进行了理论研究。我们研究了散焦、晶体倾斜和噪声的影响,发现应变的绝对误差至少应为1%-2%。模型结构包括使用分子动力学确定的表面弛豫,并且我们表明这对于正确评估图像像差引入的误差很重要。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/bd53/5656738/1acd710ecf8b/40679_2017_47_Fig1_HTML.jpg

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