Kataoka Yohei, Watanabe Takahiro, Hayashi Kyoko, Ozawa Ran, Takizawa Kazuhiro, Akiyama Hiroshi
National Institute of Health Sciences.
Japan Food Inspection Corporation.
Shokuhin Eiseigaku Zasshi. 2017;58(6):275-280. doi: 10.3358/shokueishi.58.275.
We developed and evaluated a method of quantifying chromium(VI) in mineral water (MW). After a performance evaluation, we performed a surveillance of chromium(VI) concentrations in 150 kinds of MW products purchased from markets in 2016. Recovery rates, as examined by using 150 spiked samples prepared from the purchased MW products, ranged from 93 to 107%. These results strongly suggest that the validated method is suitable for quantifying chromium(VI) in MW. Chromium(VI) was detected in 65 kinds of MW products; the detection rate was 43%. The minimum concentration of chromium(VI) was 0.0001 mg/L and the maximum was 0.0019 mg/L. The median value of chromium(VI) concentration was 0.0003 mg/L. In most of the products in which chromium(VI) was detected, the concentration ranged from 0.0001 to 0.0002 mg/L. No products were found with concentrations higher than the value (0.05 mg/L) set by the Food Sanitation Law as the specification for MW.
我们开发并评估了一种测定矿泉水中六价铬的方法。在进行性能评估后,我们对2016年从市场购买的150种矿泉水产品中的六价铬浓度进行了监测。通过使用从购买的矿泉水产品制备的150个加标样品进行检测,回收率在93%至107%之间。这些结果有力地表明,经过验证的方法适用于测定矿泉水中的六价铬。在65种矿泉水产品中检测到了六价铬;检出率为43%。六价铬的最低浓度为0.0001mg/L,最高浓度为0.0019mg/L。六价铬浓度的中值为0.0003mg/L。在大多数检测到六价铬的产品中,浓度范围为0.0001至0.0002mg/L。未发现有产品的浓度高于《食品卫生法》规定的矿泉水标准值(0.05mg/L)。