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新型烧结多层金属丝网多孔板的制备、结构表征及单轴拉伸性能

Fabrication, Structural Characterization and Uniaxial Tensile Properties of Novel Sintered Multi-Layer Wire Mesh Porous Plates.

作者信息

Duan Liuyang, Zhou Zhaoyao, Yao Bibo

机构信息

National Engineering Research Center of Near-Net-Shape Forming for Metallic Materials, School of Mechanical and Automotive Engineering, South China University of Technology, Guangzhou 510640, China.

出版信息

Materials (Basel). 2018 Jan 17;11(1):156. doi: 10.3390/ma11010156.

Abstract

There is an increasing interest in developing porous metals or metallic foams for functional and structural applications. The study of the physical and mechanical properties of porous metals is very important and helpful for their application. In this paper, a novel sintered multilayer wire mesh porous plate material (WMPPs) with a thickness of 0.5 mm-3 mm and a porosity of 10-35% was prepared by winding, pressing, rolling, and subsequently vacuum sintering them. The pore size and total size distribution in the as-prepared samples were investigated using the bubble point method. The uniaxial tensile behavior of the WMPPs was investigated in terms of the sintering temperature, porosity, wire diameter, and manufacturing technology. The deformation process and the failure mechanism under the tensile press was also discussed based on the appearance of the fractures (SEM figures). The results indicated that the pore size and total size distribution were closely related to the raw material used and the sintering temperature. For the WMPPs prepared by the wire mesh, the pore structures were inerratic and the vast majority of pore size was less than 10 μm. On the other hand, for the WMPPs that were prepared by wire mesh and powder, the pore structures were irregular and the pore size ranged from 0 μm-50 μm. The experimental data showed that the tensile strength of WMPPs is much higher than any other porous metals or metallic foams. Higher sintering temperatures led to coarser joints between wires and resulted in higher tensile strength. The sintering temperature decreased from 1330 °C to 1130 °C and the tensile strength decreased from 296 MPa to 164 MPa. Lower porosity means that there are more metallurgical joints and metallic frameworks resisting deformation per unit volume. Therefore, lower porosities exhibit higher tensile strength. An increase of porosity from 17.14% to 32.5% led to the decrease of the tensile strength by 90 MPa. The coarser wires led to a bigger contact area between the interconnecting wires, resulting in a stronger sintering neck that exhibited higher tensile strength. The wire diameter increased from 81 μm to 122 μm and the tensile strength increased from 296 MPa to 362 MPa. The fracture morphology showed that the wires experience necking deformation and ductile fracture.

摘要

开发用于功能和结构应用的多孔金属或金属泡沫正受到越来越多的关注。研究多孔金属的物理和力学性能对其应用非常重要且有帮助。本文通过缠绕、压制、轧制,随后进行真空烧结,制备了一种厚度为0.5毫米至3毫米、孔隙率为10%至35%的新型烧结多层丝网多孔板材料(WMPPs)。使用泡点法研究了制备样品中的孔径和总尺寸分布。从烧结温度、孔隙率、丝径和制造工艺方面研究了WMPPs的单轴拉伸行为。基于断裂外观(扫描电子显微镜图像)还讨论了拉伸压力下的变形过程和失效机制。结果表明,孔径和总尺寸分布与所用原材料和烧结温度密切相关。对于由丝网制备的WMPPs,孔隙结构不规则,绝大多数孔径小于10微米。另一方面,对于由丝网和粉末制备的WMPPs,孔隙结构不规则,孔径范围为0微米至50微米。实验数据表明,WMPPs的拉伸强度远高于任何其他多孔金属或金属泡沫。较高的烧结温度导致丝间接头更粗,从而导致更高的拉伸强度。烧结温度从1330℃降至1130℃,拉伸强度从296MPa降至164MPa。较低的孔隙率意味着单位体积内有更多的冶金接头和抵抗变形的金属框架。因此,较低的孔隙率表现出较高的拉伸强度。孔隙率从17.14%增加到32.5%导致拉伸强度降低90MPa。较粗的丝导致互连丝之间的接触面积更大,从而形成更强的烧结颈,表现出更高的拉伸强度。丝径从81微米增加到122微米,拉伸强度从296MPa增加到362MPa。断口形貌表明,丝经历颈缩变形和韧性断裂。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d27e/5793654/d3e40ba60953/materials-11-00156-g001.jpg

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