• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利：CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法，用中文像聊天一样搜索，搜遍4000万医学文献。AI智能推荐，让科研检索更轻松。

立即免费搜索

文件翻译

保留排版，准确专业，支持PDF/Word/PPT等文件格式，支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述，25分钟生成高质量综述，智能提取关键信息，辅助科研写作。

立即免费体验

通过在超声作用下碳与α-二醇及氢氧化钠的多相反应选择性合成富勒烯稠合二氧六环加合物。

A selective synthesis of the fullerene-fused dioxane adduct via heterogeneous reaction of C with α-diols and NaOH under ultrasonication.

作者信息

Kinzyabaeva Zemfira S, Sharipov Glus L

机构信息

Laboratory of High Energy Chemistry and Catalysis, Institute of Petrochemistry and Catalysis, Russian Academy of Sciences, 141 Prospekt Oktyabrya, Ufa 450075, Russia.

Laboratory of High Energy Chemistry and Catalysis, Institute of Petrochemistry and Catalysis, Russian Academy of Sciences, 141 Prospekt Oktyabrya, Ufa 450075, Russia.

出版信息

Ultrason Sonochem. 2018 Apr;42:119-123. doi: 10.1016/j.ultsonch.2017.11.012. Epub 2017 Nov 8.

DOI:10.1016/j.ultsonch.2017.11.012
PMID:29429652
Abstract

A novel ultrasonic-mediated approach to the synthesis of 1,9-dihydro[C-I]5,6fullerene based on the heterogeneous reaction of fullerene with α-diols and NaOH has been developed. It allows producing the fullerene derivatives with high yields and selectivity.

摘要

一种基于富勒烯与α-二醇和氢氧化钠的多相反应，通过新型超声介导方法合成1,9-二氢[C-I]5,6富勒烯的方法已被开发出来。它能够以高产率和选择性制备富勒烯衍生物。

相似文献

1
A selective synthesis of the fullerene-fused dioxane adduct via heterogeneous reaction of C with α-diols and NaOH under ultrasonication.通过在超声作用下碳与α-二醇及氢氧化钠的多相反应选择性合成富勒烯稠合二氧六环加合物。
Ultrason Sonochem. 2018 Apr;42:119-123. doi: 10.1016/j.ultsonch.2017.11.012. Epub 2017 Nov 8.
2
Sonochemical synthesis of novel C fullerene 1,4-oxathiane derivative through the intermediate fullerene radical anion.通过中间富勒烯自由基阴离子声化学合成新型C富勒烯1,4-氧硫杂环戊烷衍生物。
Ultrason Sonochem. 2020 Oct;67:105169. doi: 10.1016/j.ultsonch.2020.105169. Epub 2020 May 8.
3
Synthesis of Fullerene-Fused Dioxanes/Dioxepanes: Ferric Perchlorate-Mediated One-Step Reaction of [60]Fullerene with Diols.富勒烯稠合二氧六环/二氧杂环庚烷的合成：高氯酸铁介导的[60]富勒烯与二醇的一步反应。
J Org Chem. 2015 Jun 19;80(12):6037-43. doi: 10.1021/acs.joc.5b00360. Epub 2015 Jun 2.
4
Development of n-Type Semiconductor Based on Cyclopentene- or Cyclohexene-Fused [C60]-Fullerene Derivatives.基于环戊烯或环己烯稠合的[C60] - 富勒烯衍生物的n型半导体的开发。
J Org Chem. 2015 May 1;80(9):4638-49. doi: 10.1021/acs.joc.5b00530. Epub 2015 Apr 22.
5
Selective formation of dihydrofuran fused [60] fullerene derivatives by TEMPO mediated [3 + 2] cycloaddition of medium chain β-keto esters to C.通过TEMPO介导的中链β-酮酯与C的[3 + 2]环加成反应选择性形成二氢呋喃稠合的[60]富勒烯衍生物
RSC Adv. 2021 Sep 2;11(47):29426-29432. doi: 10.1039/d1ra03944j. eCollection 2021 Sep 1.
6
Sonochemical reaction of fullerene[C60] with several 2'-azidoethyl per-O-acetyl glycosides.
J Nanosci Nanotechnol. 2008 Jun;8(6):3136-41. doi: 10.1166/jnn.2008.091.
7
Synthesis of a water-soluble fullerene [C60] under ultrasonication.超声作用下一种水溶性富勒烯[C60]的合成。
Ultrasonics. 2004 Mar;41(9):727-30. doi: 10.1016/j.ultras.2003.12.029.
8
Iodo-controlled selective formation of pyrrolidino[60]fullerene and aziridino[60]fullerene from the reaction between C6) and amino acid esters.碘控制下由C60与氨基酸酯反应选择性生成吡咯烷基[60]富勒烯和氮丙啶基[60]富勒烯。
J Org Chem. 2004 Aug 20;69(17):5800-2. doi: 10.1021/jo0493368.
9
Palladium-catalyzed synthesis of [60]fullerene-fused benzofurans via heteroannulation of phenols.钯催化酚类的杂环化反应合成[60]富勒烯稠合苯并呋喃
Chem Commun (Camb). 2017 Feb 2;53(11):1852-1855. doi: 10.1039/c6cc09080j.
10
Synthesis and Isolation of cis-2 Regiospecific Ethylene-Tethered Indene Dimer-[70]Fullerene Adduct for Polymer Solar Cell Applications.用于聚合物太阳能电池应用的顺式-2 位区域选择性乙烯桥联茚二聚体-[70]富勒烯加合物的合成与分离。
ACS Appl Mater Interfaces. 2015 Aug 5;7(30):16676-85. doi: 10.1021/acsami.5b04351. Epub 2015 Jul 27.

引用本文的文献

1
Green and rapid preparation of long-term stable aqueous dispersions of fullerenes and endohedral fullerenes: The pros and cons of an ultrasonic probe.富勒烯和笼状富勒烯的绿色快速制备及其长期稳定水性分散体：超声探头的优缺点。
Ultrason Sonochem. 2021 May;73:105533. doi: 10.1016/j.ultsonch.2021.105533. Epub 2021 Mar 19.