Arnold F, Naumann M, Lühmann Th, Mackenzie A P, Hassinger E
Max Planck Institute for Chemical Physics of Solids, 01187 Dresden, Germany.
Rev Sci Instrum. 2018 Feb;89(2):023901. doi: 10.1063/1.5011655.
Torque magnetometry is a key method to measure the magnetic anisotropy and quantum oscillations in metals. In order to resolve quantum oscillations in sub-millimeter sized samples, piezo-electric micro-cantilevers were introduced. In the case of strongly correlated metals with large Fermi surfaces and high cyclotron masses, magnetic torque resolving powers in excess of 10 are required at temperatures well below 1 K and magnetic fields beyond 10 T. Here, we present a new broadband read-out scheme for piezo-electric micro-cantilevers via Wheatstone-type resistance measurements in magnetic fields up to 15 T and temperatures down to 200 mK. By using a two-stage superconducting-quantum interference device as a null detector of a cold Wheatstone bridge, we were able to achieve a magnetic moment resolution of Δm = 4 × 10 J/T at maximal field and 700 mK, outperforming conventional magnetometers by at least one order of magnitude in this temperature and magnetic field range. Exemplary de Haas-van Alphen measurement of a newly grown delafossite, PdRhO, was used to show the superior performance of our setup.
扭矩磁力测量法是测量金属中磁各向异性和量子振荡的关键方法。为了解析亚毫米尺寸样品中的量子振荡,人们引入了压电微悬臂梁。对于具有大费米面和高回旋质量的强关联金属,在远低于1 K的温度和超过10 T的磁场下,需要超过10的磁扭矩分辨能力。在此,我们展示了一种通过惠斯通电桥型电阻测量对压电微悬臂梁进行宽带读出的新方案,该测量可在高达15 T的磁场和低至200 mK的温度下进行。通过使用两级超导量子干涉器件作为冷惠斯通电桥的零探测器,我们能够在最大磁场和700 mK时实现Δm = 4×10 J/T的磁矩分辨率,在该温度和磁场范围内,其性能比传统磁力计至少高出一个数量级。对新生长的铜铁矿PdRhO进行的德哈斯 - 范阿尔芬测量示例展示了我们装置的卓越性能。