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热聚合条件及微波对聚甲基丙烯酸甲酯弯曲强度的影响

Effect of heat polymerization conditions and microwave on the flexural strength of polymethyl methacrylate.

作者信息

Ozkir Serhat Emre, Yilmaz Burak, Unal Server Mutluay, Culhaoglu Ahmet, Kurkcuoglu Isin

机构信息

Department of Prosthodontics, Faculty of Dentistry, Afyon Kocatepe University, Afyonkarahisar, Turkiye.

Division of Restorative Sciences and Prosthodontics, College of Dentistry, The Ohio State University, Columbus, Ohio, USA.

出版信息

Eur J Dent. 2018 Jan-Mar;12(1):116-119. doi: 10.4103/ejd.ejd_199_17.

Abstract

OBJECTIVE

The objective of this study is the effect of different heat polymerization conditions on the strength of polymethyl methacrylate (PMMA) resin base is unknown. Distinguishing one method that provides improved mechanical properties may be beneficial to the clinical success of complete and partial dentures and overdentures. The purpose of this study was to evaluate the effect of different polymerization methods on the flexural strength of a dental PMMA resin.

MATERIALS AND METHODS

Forty PMMA specimens (64 mm × 10 mm × 4 mm) were prepared with 4 different polymerization methods ( = 10); heat polymerization at 74°C for 9 h, at 100°C for 40 min, and with 620 kPa pressure at 100°C for 20 min. The remaining group of specimens was microwave polymerized at 180 W for 6 min. All specimens were thermocycled at 5°C and 55°C for 5000 times. Three-point flexure test was used to measure the flexural strength of specimens. One-way ANOVA and Tukey Honestly Significant Difference were applied to analyze the differences in flexural strengths (α = 0.05).

RESULTS

The flexural strength of heat-polymerized groups was similar. The flexural strength of microwave polymerized group was significantly different and lower than the other groups ( < 0.05).

CONCLUSION

Polymerizing conventional heat-polymerizing PMMA resin with microwave energy resulted in a significant decrease in flexural strength. The results of this study suggest that clinicians may benefit from using heat polymerization when processing PMMA denture bases instead of microvawe polymerization when tested brand is used.

摘要

目的

本研究的目的是不同热聚合条件对聚甲基丙烯酸甲酯(PMMA)树脂基托强度的影响尚不清楚。区分一种能提供改善机械性能的方法可能有利于全口义齿、局部义齿和覆盖义齿的临床成功。本研究的目的是评估不同聚合方法对牙科PMMA树脂弯曲强度的影响。

材料与方法

采用4种不同的聚合方法制备40个PMMA标本(64mm×10mm×4mm)(每组n = 10);在74°C下热聚合9小时,在100°C下热聚合40分钟,以及在100°C下620kPa压力下热聚合20分钟。其余标本组在180W下微波聚合6分钟。所有标本在5°C和55°C下进行5000次热循环。采用三点弯曲试验测量标本的弯曲强度。应用单因素方差分析和Tukey真实显著性差异分析弯曲强度的差异(α = 0.05)。

结果

热聚合组的弯曲强度相似。微波聚合组的弯曲强度有显著差异,且低于其他组(P < 0.05)。

结论

用微波能量聚合传统热聚合PMMA树脂会导致弯曲强度显著降低。本研究结果表明,在处理PMMA义齿基托时,临床医生使用热聚合可能比使用微波聚合更有益,前提是使用的是测试品牌。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4d52/5883462/88572147c599/EJD-12-116-g001.jpg

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