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3D 打印系统、后聚合和老化方案对用于打印咬合垫、模型和临时修复体的树脂弯曲强度和尺寸稳定性的影响。

Influence of 3D printing system, postpolymerization and aging protocols on resin flexural strength and dimensional stability for printing occlusal splints, models and temporary restorations.

机构信息

Department of Dentistry, Federal University of Rio Grande Do Norte (UFRN), Av. Salgado Filho, 1787, Lagoa Nova, Natal, RN, CEP: 59056-000, Brazil.

Department of Restorative Dentistry, Federal University of Paraiba (UFPB), João Pessoa, Paraíba, Brazil.

出版信息

Clin Oral Investig. 2024 Oct 19;28(11):604. doi: 10.1007/s00784-024-05998-4.

Abstract

OBJECTIVES

Investigate the effect of different postpolymerization protocols, aging, and 3D printing systems on the flexural strength (σ), dimensional stability, and roughness of resins used to fabricate occlusal splints, dental models, and temporary restorations.

MATERIAL AND METHODS

180 bars (25 × 2 x 2 mm-ISO 4049) of each type of resin (T-Temporary/Cosmos Temp, Yller; OS-Occlusal splint/Cosmos Splint, Yller; MO - Models/ Cosmos Model, Yller) were printed and divided into 12 groups (n = 15) according to the factors: "Postpolymerization" (Ctr - Control; UV - Ultraviolet oven and MW - Microwave); "Printer" (SLA- stereolithography (Forms 2/Formslab); LCD- liquid crystal display (FlashForge Foto 6.0/FlashForge)) and "Aging" (TC - 10,000 thermocycling cycles and Without). Each bar was measured with a digital caliper at 11 points before and after postpolymerization to evaluate dimensional stability. The samples were subjected to the σ test (100Kgf;1 mm/min). Data was evaluated using Three- and Two-way ANOVA, and Tukey's test (5%). Weibull analysis, Scanning Electron Microscopic and optical profilometry was performed.

RESULTS

LCD printing system and UV oven postpolymerization exhibited the highest σ (P < .05). The groups printed in SLA and post-polymerized in microwave ovens showed the greatest variations in their dimensions, for the occlusal splint resin, the OS-SLA-MW group (-4.29 ± 3.15) showed a shrinkage of 40.2%. The resins for models (3.31 ± 0.66) and temporary (-2.06 ± 1.52) showed a shrinkage of 33% and 20.6%, respectively.

CONCLUSIONS

LCD printing with UV light postpolymerization was the most effective method for resins used in occlusal splints, dental models, and temporary restorations. SLA printing with UV postpolymerization showed the most significant dimensional changes, leading to shrinkage in occlusal splint resins, while model resins and temporary restorations expanded.

CLINICAL RELEVANCE

Resins for 3D printing should ideally be post-polymerized with UV light and printed using LCD technology, as this approach results in better mechanical properties and less dimensional change compared to microwave oven post-polymerization.

摘要

目的

研究不同后聚合方案、老化和 3D 打印系统对用于制作咬合垫、牙模和临时修复体的树脂的弯曲强度(σ)、尺寸稳定性和粗糙度的影响。

材料与方法

将每种类型的树脂(T-临时/CosmosTemp,Yller;OS-咬合垫/CosmosSplint,Yller;MO-模型/CosmosModel,Yller)各制作 180 个 25x2x2mm-ISO4049 条,并根据以下因素分为 12 组(n=15):“后聚合”(Ctr-对照;UV-紫外线烤箱和 MW-微波);“打印机”(SLA-立体光固化(Forms2/Formslab);LCD-液晶显示(FlashForge Foto6.0/FlashForge))和“老化”(TC-10000 次热循环和无)。聚合后,在 11 个点处用数字卡尺测量每个条,以评估尺寸稳定性。对样品进行 σ 测试(100Kgf;1mm/min)。使用三因素和双因素方差分析以及 Tukey 检验(5%)对数据进行评估。进行威布尔分析、扫描电子显微镜和光学轮廓术。

结果

LCD 打印系统和 UV 烤箱后聚合显示出最高的 σ(P<.05)。在 SLA 中打印并在微波炉中后聚合的组显示出其尺寸的最大变化,对于咬合垫树脂,OS-SLA-MW 组(-4.29±3.15)显示出 40.2%的收缩。模型(3.31±0.66)和临时(-2.06±1.52)树脂分别收缩 33%和 20.6%。

结论

用于咬合垫、牙模和临时修复体的树脂,使用 LCD 打印和 UV 光后聚合是最有效的方法。使用 UV 后聚合的 SLA 打印显示出最显著的尺寸变化,导致咬合垫树脂收缩,而模型树脂和临时修复体膨胀。

临床意义

3D 打印用树脂理想的后聚合方法是使用紫外线光,打印方法是使用 LCD 技术,因为与微波后聚合相比,这种方法可以获得更好的机械性能和更小的尺寸变化。

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