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树脂粘结系统和氧化铝颗粒空气研磨对与氧化锆粘结强度的影响。

Effect of Resin Luting Systems and Alumina Particle Air Abrasion on Bond Strength to Zirconia.

作者信息

Grasel R, Santos M J, Rêgo Hm Chagas, Rippe M P, Valandro L F

出版信息

Oper Dent. 2018 May/Jun;43(3):282-290. doi: 10.2341/15-352-L.

Abstract

This study aimed to evaluate the effect of different primer/resin luting agent combinations and alumina air abrasion on the adhesion to zirconia. Eighty blocks (4×4×3 mm) of Lava Frame Zirconia (3M ESPE) were produced and randomly assigned into eight groups (n=10) according to two zirconia surface treatments (untreated or air abrasion with 50-μm alumina particles) and four luting systems (SU: Scotchbond Universal/RelyX Unicem 2; ZP: Z-Prime Plus/Duo-link Universal; MB: Monobond Plus/Variolink II; and AP: Alloy Primer/ED Primer II/Panavia F 2.0). After the conditioning and primer applications, resin luting agents were manipulated and applied on the zirconia, using a matrix, to form a cylinder (2 mm in diameter×2 mm high), followed by photoactivation for 40 seconds. After that, the specimens were stored in distilled water (37 °C) for 120 days and then submitted to shear bond strength testing, followed by failure mode evaluation under an optical microscope (30×). A two-way analysis of variance and Tukey test (α=0.05) were used for data analysis. Alumina air abrasion (Al) promoted higher bond values for the three luting systems, except for SU, which showed the best results without air abrasion, while with air abrasion, Al-SU, Al-ZP, and Al-MB presented higher values compared to Al-AP. We concluded that the alumina air abrasion of zirconia surfaces seemed to be dispensable for the SU group, while air abrasion (topographical alterations) enhanced the adhesion of the ZP, MB, and AP groups.

摘要

本研究旨在评估不同的底漆/树脂粘结剂组合以及氧化铝气磨对与氧化锆粘结的影响。制备了80块Lava Frame氧化锆(3M ESPE)方块(4×4×3毫米),并根据两种氧化锆表面处理方式(未处理或用50微米氧化铝颗粒进行气磨)和四种粘结系统(SU:Scotchbond Universal/RelyX Unicem 2;ZP:Z-Prime Plus/Duo-link Universal;MB:Monobond Plus/Variolink II;AP:Alloy Primer/ED Primer II/Panavia F 2.0)随机分为八组(n = 10)。在进行预处理和底漆应用后,使用模具将树脂粘结剂调配并涂覆在氧化锆上,形成一个圆柱体(直径2毫米×高2毫米),然后光固化40秒。之后,将试样在蒸馏水(37°C)中储存120天,然后进行剪切粘结强度测试,随后在光学显微镜(30倍)下评估失效模式。采用双向方差分析和Tukey检验(α = 0.05)进行数据分析。除SU组外,氧化铝气磨(Al)对其他三种粘结系统均提高了粘结值,SU组在未进行气磨时显示出最佳结果,而在进行气磨时,Al-SU、Al-ZP和Al-MB组的值高于Al-AP组。我们得出结论,氧化锆表面的氧化铝气磨对于SU组似乎是不必要的,而气磨(表面形貌改变)增强了ZP、MB和AP组的粘结力。

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