Brosius Nevin, Ward Kevin, Matsumoto Satoshi, SanSoucie Michael, Narayanan Ranga
1Department of Chemical Engineering, University of Florida, Gainesville, FL 32611 USA.
2Human Spaceflight Technology Directorate, Japan Aerospace Exploration Agency, Tsukuba, Ibaraki 305-8505 Japan.
NPJ Microgravity. 2018 May 14;4:10. doi: 10.1038/s41526-018-0044-1. eCollection 2018.
In this work, a method for the measurement of surface tension using continuous periodic forcing is presented. To reduce gravitational effects, samples are electrostatically levitated prior to forcing. The method, called Faraday forcing, is particularly well suited for fluids that require high temperature measurements such as liquid metals where conventional surface tension measurement methods are not possible. It offers distinct advantages over the conventional pulse-decay analysis method when the sample viscosity is high or the levitation feedback control system is noisy. In the current method, levitated drops are continuously translated about a mean position at a small, constant forcing amplitude over a range of frequencies. At a particular frequency in this range, the drop suddenly enters a state of resonance, which is confirmed by large executions of prolate/oblate deformations about the mean spherical shape. The arrival at this resonant condition is a signature that the parametric forcing frequency is equal to the drop's natural frequency, the latter being a known function of surface tension. A description of the experimental procedure is presented. A proof of concept is given using pure Zr and a TiZrNi alloy as examples. The results compare favorably with accepted literature values obtained using the pulse-decay method.
在这项工作中,提出了一种使用连续周期性外力来测量表面张力的方法。为了减少重力影响,在施加外力之前,样品通过静电悬浮。这种方法称为法拉第外力作用,特别适用于需要高温测量的流体,如液态金属,而传统的表面张力测量方法在这种情况下是不可行的。当样品粘度高或悬浮反馈控制系统有噪声时,它相对于传统的脉冲衰减分析方法具有明显优势。在当前方法中,悬浮液滴在一系列频率上以小的、恒定的外力振幅围绕平均位置连续平移。在该频率范围内的某个特定频率下,液滴突然进入共振状态,这通过围绕平均球形的长轴/短轴变形的大幅执行得到证实。达到这种共振状态表明参数外力频率等于液滴的固有频率,后者是表面张力的已知函数。本文介绍了实验过程。以纯Zr和TiZrNi合金为例给出了概念验证。结果与使用脉冲衰减法获得的公认文献值相比具有优势。