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不同吸附剂在生物样品 SPE 和 SPME 中的最新发展与应用。

Recent developments and applications of different sorbents for SPE and SPME from biological samples.

机构信息

Department of Chemistry, Razi University, Kermanshah, Iran.

Faculty of Chemistry, Bu-Ali Sina University, Hamedan, Iran.

出版信息

Talanta. 2018 Sep 1;187:337-347. doi: 10.1016/j.talanta.2018.05.053. Epub 2018 May 21.

DOI:10.1016/j.talanta.2018.05.053
PMID:29853056
Abstract

Solid phase extraction (SPE) and solid phase microextraction (SPME) are among the most significant sample clean-up and pretreatment techniques, which have attracted a considerable interest in the pre-concentration and determination of a wide variety of analytes in biological, pharmaceutical, environmental, industrial and food samples. The purpose of this review article is to focus on the latest advancements and applications of SPE and SPME methods based on new nanomaterial adsorbents for separation, concentration and determination of different analytes in biological media. To this end, some sorbents such as metal organic frameworks, molecularly/ion-imprinted polymers, carbon nanotubes, magnetic nanoparticles, graphene and graphene oxide, and metallic nanoparticles are discussed here.

摘要

固相萃取(SPE)和固相微萃取(SPME)是最重要的样品净化和预处理技术之一,它们在生物、制药、环境、工业和食品样品中对各种分析物的预浓缩和测定引起了相当大的兴趣。本文的目的是侧重于基于新型纳米材料吸附剂的 SPE 和 SPME 方法的最新进展和应用,用于分离、浓缩和测定生物介质中的不同分析物。为此,本文讨论了一些吸附剂,如金属有机框架、分子/离子印迹聚合物、碳纳米管、磁性纳米粒子、石墨烯和氧化石墨烯以及金属纳米粒子。

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