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从水果中提取的多糖的中性糖的气相色谱-电子轰击质谱鉴定数据

GC-EI-MS identification data of neutral sugars of polysaccharides extracted from fruit.

作者信息

Hammi Khaoula Mkadmini, Hammami Majdi, Rihouey Christophe, Le Cerf Didier, Ksouri Riadh, Majdoub Hatem

机构信息

Laboratoire des Plantes Aromatiques et Médicinales (LPAM), Centre de Biotechnologie de Borj- Cédria, BP 901, 2050 Hammam-lif, Tunisia.

Université de Monastir, Laboratoire des Interfaces et des Matériaux Avancés (LIMA), Faculté des Sciences de Monastir, Bd. de l'environnement, 5019 Monastir, Tunisia.

出版信息

Data Brief. 2018 Feb 10;18:680-683. doi: 10.1016/j.dib.2018.01.085. eCollection 2018 Jun.

Abstract

Gas chromatography coupled to mass spectrometer (GC-MS) was used to identify and to quantify neutral sugars that constitute the water soluble polysaccharides from fruit. The trimethylsilyl (TMS) method was successfully used for derivatization of the monosaccharides units of extracted polysaccharides that were released by hydrolysis method. Sugars were identified based on their retention times compared with those of standards and the NIST MS Spectral Library. All sugars were quantified in TIC (Total Ion Current) mode using calibration curves. Data is related to "Optimization extraction of polysaccharide from Tunisian fruit by response surface methodology: Composition and antioxidant activity" (Mkadmini Hammi et al., 2016) [1].

摘要

气相色谱-质谱联用仪(GC-MS)用于鉴定和定量构成水果水溶性多糖的中性糖。三甲基硅烷基(TMS)法成功用于衍生化通过水解法释放的提取多糖的单糖单元。通过与标准品的保留时间以及NIST质谱图库进行比较来鉴定糖类。所有糖类均使用校准曲线在总离子流(TIC)模式下进行定量。数据与“采用响应面法优化突尼斯水果多糖的提取:组成与抗氧化活性”(Mkadmini Hammi等人,2016年)[1]相关。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/78f0/5995744/c0652d9a4dc8/gr1.jpg

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