J Adhes Dent. 2018;20(2):107-112. doi: 10.3290/j.jad.a40298.
To evaluate the effect of cusp inclination and light-curing time on the microshear bond strength (μSBS) between zirconia and a dual-cure self-adhesive composite cement and zirconia.
Forty U-shaped specimens with angled surfaces, simulating different cusp inclinations (0 degrees, 20 degrees, and 30 degrees), were fabricated from zirconia blocks (Zenostar, Wieland). The specimens were randomly divided into two groups (n = 20) according to different light-curing times of the adhesive composite cements (20 s and 40 s). Three polyethylene tubes filled with a dual-curing self-adhesive composite cement (Multilink Speed, Ivoclar Vivadent) were bonded to the surfaces of each specimen with light-curing times of 20 s and 40 s. The μSBS was tested using a universal testing machine with a crosshead speed of 0.5 mm/min. Failure analysis was performed. Two-way ANOVA (cusp inclination and light-curing time) followed by two independent samples t-test were used for statistical analyses (α = 0.05).
The composite cement showed various bond strengths to angled zirconia surfaces (7.07 ± 1.69 to 13.91 ± 3.11 MPa). The μSBS between composite cement and 0-degree zirconia surfaces was statistically higher than that of 20- and 30-degree zirconia surfaces. The composite cement light cured for 40 s showed nonsignificantly higher μSBS than did the composite cement cured for 20 s. Adhesive failure was the most common failure mode.
Cusp inclination affected bond strength between the dual-curing self-adhesive composite cement and zirconia.
评估牙尖斜度和光照时间对氧化锆与双固化自粘接复合树脂粘结剂及氧化锆之间微剪切粘结强度(μSBS)的影响。
从氧化锆块(泽尼思塔,威兰德)中制作 40 个具有斜面的 U 形样本,模拟不同的牙尖斜度(0 度、20 度和 30 度)。根据粘结剂复合树脂的不同光照时间(20 秒和 40 秒),将样本随机分为两组(n=20)。用光照时间为 20 秒和 40 秒的 3 个聚乙烯管将双固化自粘接复合树脂(Multilink Speed,义获嘉伟瓦登特)粘接到每个样本的表面。用万能试验机以 0.5mm/min 的十字头速度测试 μSBS。进行失效分析。采用双因素方差分析(牙尖斜度和光照时间),再进行两个独立样本 t 检验进行统计学分析(α=0.05)。
复合树脂对有斜面的氧化锆表面的粘结强度不同(7.07±1.69~13.91±3.11 MPa)。复合树脂与 0 度氧化锆表面之间的 μSBS 明显高于 20 度和 30 度氧化锆表面。40 秒光照固化的复合树脂的 μSBS 明显高于 20 秒光照固化的复合树脂。粘结破坏是最常见的失效模式。
牙尖斜度影响双固化自粘接复合树脂与氧化锆之间的粘结强度。