Górka Jacek, Czupryński Artur, Żuk Marcin, Adamiak Marcin, Kopyść Adam
Department of Welding Engineering, Silesian University of Technology, Konarskiego 18A, 44-100 Gliwice, Poland.
Institute of Engineering Materials and Biomaterials, Silesian University of Technology, Konarskiego 18A, 44-100 Gliwice, Poland.
Materials (Basel). 2018 Jul 10;11(7):1184. doi: 10.3390/ma11071184.
Presented in this work are the properties and structure characteristics of MMA (Manual Metal Arc) deposited nanocrystalline coatings (Fe-Cr-Nb-B) applied to an iron nanoalloy matrix on an S355N steel substrate in relation to selected construction materials resistant to abrasive wear currently used in industry. The obtained overlay welds were subjected to macro and microscopic metallographic examinations; grain size was determined by X-ray diffraction (XRD), and chemical composition of precipitates was determined by energy-dispersive X-ray spectroscopy (EDS) during scanning electron microscopy (SEM). The size of the crystalline grains of the Fe-Cr-Nb-B nanocrystalline microstructure was analyzed using an Xpert PRO X-ray diffractometer. Analysis of the test results of the obtained layers of arc-welded Fe-Cr-Nb-B-type alloy confirmed that the obtained layers are made of crystallites with a size of 20 nm, which classifies these layers as nanocrystalline. The obtained nanocrystalline coatings were assessed by hardness and with the use of metal-mineral abrasion testing. The results of the coatings' properties tests were compared to HARDOX 400 alloy steel.
本研究展示了在S355N钢基体上的铁纳米合金基体上应用的MMA(手工金属电弧)沉积纳米晶涂层(Fe-Cr-Nb-B)的性能和结构特征,与目前工业上使用的选定耐磨建筑材料相关。对获得的堆焊层进行了宏观和微观金相检验;通过X射线衍射(XRD)测定晶粒尺寸,并在扫描电子显微镜(SEM)期间通过能量色散X射线光谱(EDS)测定析出物的化学成分。使用Xpert PRO X射线衍射仪分析Fe-Cr-Nb-B纳米晶微观结构的晶粒尺寸。对获得的电弧焊Fe-Cr-Nb-B型合金层的测试结果分析证实,获得的层由尺寸为20nm的微晶组成,这将这些层归类为纳米晶。通过硬度和金属-矿物磨损测试对获得的纳米晶涂层进行评估。将涂层性能测试结果与HARDOX 400合金钢进行比较。