Zhang Li-jiao, Huang Jin-chu, Lin Hong-jian, Lai Wan-chang, Li Dan, Wang Guang-xi, Gu Run-qiu, Lai Yu-rou, Yan Rong-hui, Wang Gang
Guang Pu Xue Yu Guang Pu Fen Xi. 2016 Apr;36(4):1127-32.
The contents of radionuclides uranium, thorium and potassium in the sedimentary rocks mainly depend on the contents of clay in the rocks. And the content of clay is the main basis for distinguishing types of sedimentary rock. Therefore, the value of specific activity or content of uranium, thorium and potassium can be as the quantitative index to distinguish sedimentary rock type. The specific activity or content of radionuclides uranium, thorium and potassium with the method of low-background gamma spectrometry can distinguish the type of rock quickly and accurately. Because of the influence of geometry, mass and moisture content in the sample, the accuracy of distinguishing types of rocks is influenced. This paper makes a theoretical discussion and experimental verification on the influence of mass and moisture content on the results of low-background gamma spectrometry. Results show that there is a linear relationship between (cps) of characteristic peak of all radionuclides and the mass of sample while different energy ranges and lithologies have different linear coefficient and trend fitting degree; The moisture content which is no more than 10%(while collecting samples, the moisture content is no more than 10%) has a little influence on the measurement results( the change values are within the twice standard deviation), so the moisture content which has no significant influence on the accuracy of distinguishing types of sedimentary rock using the method of low-background gamma spectrometry could not be considered. The distinguishing experiment of drilling cuttings samples collected from one oil and gas exploration area in Shanxi Dingbian is done. By the mass correction of the measured data, normalized (cps) ((cps) of per unit mass) of uranium, thorium and potassium channel can only roughly divide the types of sedimentary rocks. Therefore, synthetic distinguishing mode is established with (cps) of combination peak of characteristic peak of uranium, thorium and potassium. The type of rocks is further subdivided, and the distinguishing accuracy is more than 75%.
沉积岩中放射性核素铀、钍和钾的含量主要取决于岩石中黏土的含量。而黏土含量是区分沉积岩类型的主要依据。因此,铀、钍和钾的比活度值或含量可作为区分沉积岩类型的定量指标。采用低本底γ能谱法测量放射性核素铀、钍和钾的比活度或含量,能够快速、准确地鉴别岩石类型。由于样品的几何形状、质量和含水量的影响,使得岩石类型鉴别精度受到影响。本文针对质量和含水量对低本底γ能谱测量结果的影响进行了理论探讨和实验验证。结果表明,各放射性核素特征峰计数率(cps)与样品质量之间存在线性关系,不同能量区间及岩性的线性系数和趋势拟合度不同;含水量不超过10%(采样时含水量不超过10%)对测量结果影响较小(变化值在两倍标准差范围内),故可不考虑含水量对采用低本底γ能谱法鉴别沉积岩类型准确性的显著影响。对取自陕西定边某油气勘探区的钻井岩屑样品进行了鉴别实验。通过对测量数据进行质量校正,铀、钍和钾道的归一化计数率(cps)(单位质量的cps)只能大致划分沉积岩类型。因此,建立了铀、钍和钾特征峰组合峰计数率(cps)的综合鉴别模式,进一步细分了岩石类型,鉴别准确率大于75%。