Zhang Yuan, Wang Jiaming, Abudukeremu Hannikezi, Nizamidin Patima, Abliz Shawket, Yimit Abliz
College of Chemistry and Chemical Engineering, Xinjiang University.
Anal Sci. 2018 Dec 10;34(12):1385-1391. doi: 10.2116/analsci.18P226. Epub 2018 Aug 31.
In this work, sodium dodecyl benzene sulfonate (SDBS) was used as a dispersing agent; a WO nanoparticle suspension was used as a sensing material. The SDBS-WO thin film/Sn-doped glass optical waveguide sensor element was prepared by spin coating. The sensing material was characterized by Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), and field-emission scanning electron microscopy (FESEM). The gas-sensing characteristics of the fabricated sensors were studied at room temperature for various gases. The experimental results indicate that the sensor exhibited a high selective response toward SO and HS and a low detection limit of 10 ppb to SO and HS. The response/recovery times for SO and HS were 2/23 and 2/18 s. However, during an electrochemical gas-sensing performance test of the SDBS-WO film at room temperature, the results indicated that the trend of the variation in resistance was consistent with the variation in the output light.
在本工作中,使用十二烷基苯磺酸钠(SDBS)作为分散剂;使用WO纳米颗粒悬浮液作为传感材料。通过旋涂制备了SDBS-WO薄膜/掺锡玻璃光波导传感器元件。采用傅里叶变换红外光谱(FTIR)、X射线衍射(XRD)和场发射扫描电子显微镜(FESEM)对传感材料进行了表征。在室温下研究了所制备传感器对各种气体的气敏特性。实验结果表明,该传感器对SO和HS表现出高选择性响应,对SO和HS的检测下限低至10 ppb。对SO和HS的响应/恢复时间分别为2/23和2/18 s。然而,在室温下对SDBS-WO薄膜进行电化学气敏性能测试时,结果表明电阻变化趋势与输出光的变化一致。