Chen Tijun, Geng Libo, Qin He, Gao Min
State Key Laboratory of Advanced Processing and Recycling of Nonferrous Metals, Lanzhou University of Technology, Lanzhou 730050, China.
Materials (Basel). 2018 Sep 13;11(9):1718. doi: 10.3390/ma11091718.
A novel core-shell-structured Ti-(Al-Si-Ti) particle (Ti-(Al-Si-Ti)) reinforced A356 matrix composite was fabricated by a new method, powder thixoforming, which combines the merits of both powder metallurgy and semisolid thixoforming. The effects of reheating temperature on the microstructure and tensile properties of the resulting composite were investigated. The results indicated that the thickening of the Al-Si-Ti compound shells, with rising the reheating temperature, significantly enhanced the strengthening role, but the fracture and peeling of the shells, at higher than 600 °C, impaired the strengthening effect. The composite formed at 600 °C had a favorable tensile elongation of 8.3% besides high tensile strengths. During tensile testing, the Ti@(Al-Si-Ti) frequently fractured across the Ti cores and occasionally cracked around the Ti cores, but preferentially fractured between the outer cracked shells and the inner cores for the composites thixoformed at higher than 600 °C. The delayed formation of cracks in the Ti-(Al-Si-Ti) and the small size of the cracks contributed to ductility improvement. The MSL model, modified according to the Ti@(Al-Si-Ti) characteristics, was essentially suitable for predicting the yield strength of such composites. The largest contribution to the strength was resulted from solid solution strengthening of Ti element, but the strengthening role from geometrically necessary dislocations was significantly improved as the reheating temperature rose from 590 °C to 600 °C.
采用一种新方法——粉末触变成形法制备了一种新型核壳结构的Ti-(Al-Si-Ti)颗粒增强A356基复合材料,该方法兼具粉末冶金和半固态触变成形的优点。研究了再加热温度对所得复合材料微观结构和拉伸性能的影响。结果表明,随着再加热温度升高,Al-Si-Ti复合壳层增厚显著增强了强化作用,但在高于600℃时壳层的断裂和剥落削弱了强化效果。在600℃形成的复合材料除具有高拉伸强度外,还具有8.3%的良好拉伸伸长率。在拉伸试验过程中,Ti@(Al-Si-Ti)经常在Ti核处断裂,偶尔在Ti核周围开裂,但对于在高于600℃触变成形的复合材料,优先在外部开裂壳层与内部核之间断裂。Ti-(Al-Si-Ti)中裂纹的延迟形成以及裂纹的小尺寸有助于改善延展性。根据Ti@(Al-Si-Ti)特性修正的MSL模型基本适用于预测此类复合材料的屈服强度。对强度贡献最大的是Ti元素的固溶强化,但随着再加热温度从590℃升至600℃,几何必需位错的强化作用显著增强。