Jarupoom Pakpoom, Jaita Pharatree, Manotham Supalak, Phatungthane Thanatep, Chokethawai Komsanti, Randorn Chamnan, Rujijanagul Gobwute
Department of Industrial Engineering, Faculty of Engineering, Rajamangala Univerisity of Technology Lanna, Chiang Mai, 50300, Thailand.
Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai, 50200, Thailand.
J Nanosci Nanotechnol. 2019 Mar 1;19(3):1276-1282. doi: 10.1166/jnn.2019.16165.
The (BaZrTiO₃)/(BaFeO); (BZT/BF) ( = 0, 0.1, 0.5 and 1 mol%) ceramics have been prepared via a solid state reaction process. Effects of BF content on the physical, microstructural, magnetic and electrical properties have been systematically investigated. High density sintered specimens (5.65-5.74 g/cm³) are obtained for all compositions. SEM micrographs show a decrease of grain size value when BF is added. Examination of the dielectric spectra show that the two phase-transition temperatures as observed for pure BZT, merges into a single phase-transition temperature for the added-samples. The addition of BF also improves the magnetic behavior ( hysteresis loops) of BZT ceramic and resultes in slight changes in ferroelectric properties. The maximum of remanent magnetization () of 7.19 emu/g is obtained for the 1 mol% sample.
通过固态反应法制备了（BaZrTiO₃）/（BaFeO）；（BZT/BF）（摩尔百分比=0、0.1、0.5和1%）陶瓷。系统研究了BF含量对其物理、微观结构、磁性和电学性能的影响。所有成分均获得了高密度烧结试样（5.65 - 5.74 g/cm³）。扫描电子显微镜图像显示，添加BF后晶粒尺寸值减小。介电谱研究表明，纯BZT中观察到的两个相变温度，在添加样品中合并为一个单一的相变温度。BF的添加还改善了BZT陶瓷的磁性能（磁滞回线），并导致铁电性能略有变化。1 mol%样品的剩余磁化强度（）最大值为7.19 emu/g。
