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疲劳承载能力和黏结剂黏合的氧化钇稳定四方氧化锆多晶全瓷简化修复体的存活率。

Load-bearing capacity under fatigue and survival rates of adhesively cemented yttrium-stabilized zirconia polycrystal monolithic simplified restorations.

机构信息

Faculty of Odontology, Federal University of Santa Maria, Santa Maria, Rio Grande do Sul, Brazil.

School of Dentistry, Meridional Faculty - IMED, Passo Fundo, Rio Grande do Sul, Brazil.

出版信息

J Mech Behav Biomed Mater. 2019 Feb;90:673-680. doi: 10.1016/j.jmbbm.2018.11.009. Epub 2018 Nov 12.

Abstract

This study evaluated the fatigue failure load, number of cycles for failure and survival probability of 2nd and 3rd generation yttrium-stabilized zirconia (YSZ) adhesively cemented to a dentin analogue substrate. Disc-shaped specimens (n = 10; Ø = 10 mm; thickness = 1.0 mm) were produced from four 2nd generation YSZs (Lava Plus, 3M ESPE; Vita In-Ceram YZ-HT, VITA Zahnfabrik; Zirlux FC, Ivoclar Vivadent; Katana ML-HT, Kuraray) and two 3rd generation YSZs (Katana UTML and Katana STML, Kuraray). Each YSZ disc was adhesively cemented (Multilink Automix System) onto its dentin analogue pair (epoxy resin, Ø = 10 mm; thickness = 2.5 mm). Fatigue tests were conducted through step-stress approach (load ranging from 400 to 2600 N; step-size of 200 N; 20,000 cycles per step, 20 Hz) and the obtained data were analyzed using Kaplan Meier and Mantel-Cox tests. Surface topography and phase transformation (m-, t-, and c-phases) inspections after particle air-abrasion of the YSZs were performed, as well as fractographic analysis of the failed specimens. Second-generation zirconia materials presented higher fatigue failure load, number of cycles for failure, and survival probability than 3rd generation. Similar topographical characteristics of the YSZs could be noted. Phase transformation (t- to m-phase) after YSZ air-abrasion was only observed for 2nd generation materials. All failures started from the surface/sub-surface defects located at the cementation interface. 2nd generation zirconia presented higher load-bearing capacity under cyclic loading than 3rd generation materials.

摘要

本研究评估了第二代和第三代钇稳定氧化锆(YSZ)在黏结到牙本质模拟基底上时的疲劳失效载荷、失效循环数和存活率。从四种第二代 YSZ(Lava Plus,3M ESPE;Vita In-Ceram YZ-HT,VITA Zahnfabrik;Zirlux FC,Ivoclar Vivadent;Katana ML-HT,Kuraray)和两种第三代 YSZ(Katana UTML 和 Katana STML,Kuraray)中制作出圆盘形试件(n=10;Ø=10mm;厚度=1.0mm)。每个 YSZ 圆盘都用 Multilink Automix System 黏结到其牙本质模拟对(环氧树脂,Ø=10mm;厚度=2.5mm)上。疲劳试验采用逐步应力法(载荷范围为 400 至 2600N;步长为 200N;每步 20,000 次循环,20Hz)进行,所得数据用 Kaplan-Meier 和 Mantel-Cox 检验进行分析。对 YSZ 进行颗粒喷砂后,进行了表面形貌和相转变(m、t 和 c 相)检查,以及对失效试件的断口分析。与第三代相比,第二代氧化锆材料的疲劳失效载荷、失效循环数和存活率更高。YSZ 的表面形貌特征也相似。仅观察到第二代 YSZ 喷砂后发生了相转变(t 相向 m 相)。所有失效均始于黏结界面处的表面/次表面缺陷。在循环载荷下,第二代氧化锆的承载能力高于第三代材料。

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