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厚边框会降低用于氧化锆全瓷修复体的饰面陶瓷的断裂韧性。

A thick frame decreases the fracture toughness of veneering ceramics used for zirconia-based all-ceramic restorations.

机构信息

Division of Molecular and Regenerative Prosthodontics, Tohoku University Graduate School of Dentistry, Sendai, Japan; Volpe Research Center, ADA Foundation, Gaithersburg, MD, USA.

Division of Molecular and Regenerative Prosthodontics, Tohoku University Graduate School of Dentistry, Sendai, Japan; Liaison Center for Innovative Dentistry, Tohoku University Graduate School of Dentistry, Sendai, Japan; Division of Fixed Prosthodontics, Meikai University School of Dentistry, Sakado, Japan.

出版信息

J Prosthodont Res. 2019 Apr;63(2):184-192. doi: 10.1016/j.jpor.2018.11.007. Epub 2018 Dec 20.

Abstract

PURPOSE

To investigate the influence of firing condition and thickness of a yttria-stabilized tetragonal zirconia polycrystal (Y-TZP) frame on the fracture toughness of veneering ceramics.

METHODS

Layering and pressable ceramics without frames or on 0.8- and 1.2-mm-thick Y-TZP frames were fired with 5 schedules (normal and 4 customized conditions). The fracture toughness of the ceramics was measured at 0.5-2.5mm from the frame by the indentation fracture method. Crystal structures at the measurement points were evaluated by X-ray diffraction (XRD) and scanning electron microscopy (SEM).

RESULTS

Under customized firing conditions, the fracture toughness of the layering ceramic significantly decreased, particularly near the frame. Use of a 1.2-mm-thick frame significantly decreased the fracture toughness of both layering and pressable ceramics compared to ceramics without the frame. The decreased fracture toughness only occurred close (0.5 and 1.0mm) to the frame. XRD analysis showed identical diffraction patterns between points near and far from the frame, suggesting that the decreased fracture toughness was not due to crystal defects or impurities. SEM revealed many microcracks and large crystals in layering ceramic near the 1.2-mm-thick frame, possibly resulting from the thermal properties of the zirconia frame, such as large heat capacity and low thermal conductivity.

CONCLUSIONS

Modification of the firing conditions from the manufacturer's instructions and inclusion of a thick Y-TZP frame decreased the fracture toughness of veneering ceramics at the interface, suggesting that a thick frame would pose a potent fracture risk in veneering ceramics used for zirconia-based all-ceramic restorations.

摘要

目的

研究烧成条件和氧化钇稳定四方氧化锆多晶(Y-TZP)边框厚度对饰瓷断裂韧性的影响。

方法

无框或 0.8 和 1.2mm 厚 Y-TZP 框的分层和可压制陶瓷采用 5 种烧成方案(常规和 4 种定制条件)进行烧成。通过压痕断裂法在距边框 0.5-2.5mm 处测量陶瓷的断裂韧性。通过 X 射线衍射(XRD)和扫描电子显微镜(SEM)评估测量点的晶体结构。

结果

在定制烧成条件下,分层陶瓷的断裂韧性显著降低,尤其是靠近边框处。与无框陶瓷相比,使用 1.2mm 厚的边框会显著降低分层和可压制陶瓷的断裂韧性。降低的断裂韧性仅发生在靠近边框的位置(0.5 和 1.0mm)。XRD 分析表明,靠近和远离边框的点之间具有相同的衍射图案,表明降低的断裂韧性不是由于晶体缺陷或杂质引起的。SEM 显示,在靠近 1.2mm 厚边框的分层陶瓷中存在许多微裂纹和大晶体,这可能是由于氧化锆边框的热性能所致,例如大的热容和低导热性。

结论

从制造商的说明修改烧成条件并包含厚的 Y-TZP 边框会降低饰瓷在界面处的断裂韧性,这表明在用于氧化锆基全瓷修复体的饰瓷中,厚边框会构成潜在的断裂风险。

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