Department of Mechanical Engineering, J.S.P.M.'S Rajarshi Shahu College of Engineering, Savitribai Phule Pune University, Pune, Maharashtra, India.
Department of Mechanical Engineering, College of Engineering, Savitribai Phule Pune University, Pune, Maharashtra, India.
Mater Sci Eng C Mater Biol Appl. 2019 Apr;97:264-274. doi: 10.1016/j.msec.2018.12.029. Epub 2018 Dec 11.
TiNi (atomic %) shape memory alloy (SMA) is a unique class of smart materials because of its unbeatable property. It plays a very important role in the construction of novel orthopedic implants, because of its lower Young's modulus compared to other biomedical implant materials, Conventional machining of Ti-Ni yields poor surface finish and low dimensional accuracy of the machined components. Wire electro-discharge machining (WEDM) can achieve high dimensional accuracy, but its thermal nature causes great concern regarding surface integrity for biocompatibility application of Ti-Ni material. Therefore, it is necessary to investigate the surface morphology and non-toxic, non-hazardous surface conductive to the human body. Hence, WEDM of Ti-Ni can be used. Shape memory effect (SME) of SMA was achieved by subsequent heat treatment processes which include annealing followed by ageing. For manufacturing the Ti-Ni implants, a WEDM optimized process has been used and various performance attributes such as material removal rate (MRR), surface roughness (SR), surface topography, metallurgical changes, recast layer, micro-hardness, residual stresses and shape recovery ability of the machined components have been evaluated, so as to obtain high biocompatibility of machined surface. The minimum surface roughness with consistency, suitable surface integrity parameters like less deposition of material, minimum recast layers thickness, consentaneous amount of surface hardness and less affecting subsurface residual stresses have been determined for validated experiment with an increase in wire feed. MRR increases with increase in wire feed. SR decreases with increase in wire feed due to enhanced splashing of molten material. Shape recovery ability near wire electro-discharge machined surface has been investigated from the biocompatible point of view. Heat treatment like annealing is found to be the most suitable process to recover shape memory effect of WEDMed samples.
TiNi(原子%)形状记忆合金(SMA)是一类独特的智能材料,因为它具有无与伦比的性能。由于其杨氏模量比其他生物医学植入材料低,因此在新型骨科植入物的构建中起着非常重要的作用。与其他生物医学植入材料相比,传统的 Ti-Ni 加工方法会导致表面光洁度差,加工部件的尺寸精度低。线放电加工(WEDM)可以实现高精度,但由于其热特性,对 Ti-Ni 材料的生物相容性应用非常关注表面完整性。因此,有必要研究表面形貌和对人体无毒、无害的表面导电性。因此,可以使用 WEDM 对 Ti-Ni 进行加工。SMA 的形状记忆效应(SME)是通过后续的热处理工艺实现的,包括退火和时效。为了制造 Ti-Ni 植入物,采用了优化的 WEDM 工艺,并评估了各种性能特性,例如材料去除率(MRR)、表面粗糙度(SR)、表面形貌、金相变化、再铸层、显微硬度、残余应力和加工部件的形状恢复能力,以获得高生物相容性的加工表面。在增加线速度的情况下,确定了具有一致性的最小表面粗糙度、合适的表面完整性参数,例如材料沉积减少、最小再铸层厚度、表面硬度一致和减少对亚表面残余应力的影响。随着线速度的增加,MRR 增加。由于熔融材料飞溅增强,SR 随线速度的增加而减小。从生物相容性的角度研究了线放电加工表面附近的形状恢复能力。发现退火等热处理是恢复 WEDMed 样品形状记忆效应的最适合工艺。