Zhu Ziliang, Guo Dengji, Xu Jiao, Lin Jianjun, Lei Jianguo, Xu Bin, Wu Xiaoyu, Wang Xujin
Institute of Semiconductor Manufacturing Research, Shenzhen University, Nan-hai Ave 3688, Shenzhen 518060, China.
Guangdong Provincial Key Laboratory of Micro/Nano Optomechatronics Engineering, College of Mechatronics and Control Engineering, Shenzhen University, Nan-hai Ave 3688, Shenzhen 518060, China.
Micromachines (Basel). 2020 Nov 20;11(11):1018. doi: 10.3390/mi11111018.
Titanium-nickel shape memory alloy (SMA) has good biomedical application value as an implant. Alloy corrosion will promote the release of toxic nickel ions and cause allergies and poisoning of cells and tissues. With this background, surface modification of TiNi SMAs using TiC-powder-assisted micro-electrical discharge machining (EDM) was proposed. This aims to explore the effect of the electrical discharge machining (EDM) parameters and TiC powder concentration on the machining properties and surface characteristics of the TiNi SMA. It was found that the material removal rate (MRR), surface roughness, and thickness of the recast layer increased with an increase in the discharge energy. TiC powder's addition had a positive effect on increasing the electro-discharge frequency and MRR, reducing the surface roughness, and the maximum MRR and the minimum surface roughness occurred at a mixed powder concentration of 5 g/L. Moreover, the recast layer had good adhesion and high hardness due to metallurgical bonding. XRD analysis found that the machined surface contains CuO, TiO, and TiC phases, contributing to an increase in the surface microhardness from 258.5 to 438.7 HV, which could be beneficial for wear resistance in biomedical orthodontic applications.
钛镍形状记忆合金(SMA)作为一种植入物具有良好的生物医学应用价值。合金腐蚀会促进有毒镍离子的释放,导致细胞和组织过敏及中毒。在此背景下,提出了采用TiC粉末辅助微电火花加工(EDM)对TiNi形状记忆合金进行表面改性。这旨在探究电火花加工(EDM)参数和TiC粉末浓度对TiNi形状记忆合金加工性能和表面特性的影响。研究发现,材料去除率(MRR)、表面粗糙度和重铸层厚度随放电能量的增加而增加。添加TiC粉末对提高放电频率和材料去除率、降低表面粗糙度有积极作用,在混合粉末浓度为5 g/L时出现最大材料去除率和最小表面粗糙度。此外,由于冶金结合,重铸层具有良好的附着力和高硬度。XRD分析发现,加工表面含有CuO、TiO和TiC相,有助于将表面显微硬度从258.5 HV提高到438.7 HV,这对生物医学正畸应用中的耐磨性可能有益。