State Key Laboratory of Oral Diseases, National Clinical Research Center for Oral Diseases, West China Hospital of Stomatology, Sichuan University, Chengdu, China; Shanghai Putuo District Eye & Tooth Disease Control and Prevention Hospital, Shanghai, China.
State Key Laboratory of Oral Diseases, National Clinical Research Center for Oral Diseases, West China Hospital of Stomatology, Sichuan University, Chengdu, China.
J Dent. 2019 Apr;83:40-49. doi: 10.1016/j.jdent.2019.02.004. Epub 2019 Feb 20.
To investigate the wear mechanisms and evolution of damage in tooth enamel-resin composite bonded interfaces caused by sliding contact, and to develop an understanding of interface degradation from a tribological viewpoint that supports clinical recommendations for improving interface integrity.
Reciprocating wear tests were performed on bonded interface samples involving commercial resin composite (Tetric N Ceram Bulk Fill), resin cement (Rely X U200) and tooth enamel using the ball-on-flat configuration. The bonded samples were subjected up to 5 × 10 cycles of sliding contact, and the wear depth and wear track morphology were characterized after increments using white light interferometry and scanning electron microscopy, respectively. Optical microscopy was also used to evaluate cracks and their propagation in the samples.
In the early stages of sliding contact, wear evolved most rapidly at the interface, followed by the enamel and the resin composite. Gradually, the difference between the wear depth at the interface and other areas decreased. Furthermore, cracks and brittle fracture appeared in the enamel during the early stages of wear, adjacent to the interface. With continuing cyclic loading, enamel wear manifested primarily as ploughs, with discontinuous pits and peeled material. Cracking decreased to only a few cracks extending to the inner enamel and parallel to the interface.
Cracking and damage occurred in the enamel during the early stages of sliding contact and accelerated by poor margin finishing. Cracks caused by wear under sliding contact could be one of the reasons for secondary caries and tooth discoloration.
研究滑动接触引起的牙釉质-树脂复合材料结合界面的磨损机制和损伤演变,从摩擦学角度了解界面降解,为改善界面完整性提供临床建议。
采用球-盘配置对涉及商业树脂复合材料(Tetric N Ceram Bulk Fill)、树脂水门汀(Rely X U200)和牙釉质的结合界面样品进行往复磨损试验。将结合样品进行高达 5×10 次的滑动接触,分别采用白光干涉法和扫描电子显微镜对增量后的磨损深度和磨损轨迹形貌进行了表征。还采用光学显微镜评估了样品中的裂纹及其扩展。
在滑动接触的早期阶段,界面处的磨损演化最快,其次是牙釉质和树脂复合材料。逐渐地,界面处和其他区域之间的磨损深度差异减小。此外,在磨损的早期阶段,牙釉质中出现了裂纹和脆性断裂,靠近界面。随着循环加载的继续,牙釉质磨损主要表现为犁沟,伴有不连续的凹坑和剥落的材料。裂纹减少到只有几条延伸到内釉质并与界面平行的裂纹。
在滑动接触的早期阶段,牙釉质中发生了裂纹和损伤,这是由于边缘修整不良而加速的。滑动接触下磨损引起的裂纹可能是继发龋和牙齿变色的原因之一。