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一种灵活的流变仪设计,用于在宽频率范围内测量软固体的粘弹性响应。

A flexible rheometer design to measure the visco-elastic response of soft solids over a wide range of frequency.

作者信息

Rolley Etienne, Snoeijer Jacco H, Andreotti Bruno

机构信息

Laboratoire de Physique de l'Ecole normale supérieure, ENS, Université PSL, CNRS, Sorbonne Université, Université Paris-Diderot, Sorbonne Paris Cité, Paris, France.

Physics of Fluids Group, Faculty of Science and Technology, University of Twente, P.O. Box 217, 7500 AE Enschede, The Netherlands.

出版信息

Rev Sci Instrum. 2019 Feb;90(2):023906. doi: 10.1063/1.5064599.

Abstract

We present a flexible setup for determining the rheology of visco-elastic materials which is based on the mechanical response of a magnet deposited at the surface of a slab of material and excited electromagnetically. An interferometric measurement of the magnet displacement allows one to reach an excellent accuracy over a wide range of frequency. Except for the magnet, there is no contact between the material under investigation and the apparatus. At low frequency, inertial effects are negligible so that the mechanical response, obtained through a lock-in amplifier, directly gives the material complex modulus. At high frequency, damped waves are emitted and the rheology must be extracted numerically from a theoretical model. To validate the design, the instrument was used to measure the rheology of a test polydimethylsiloxane gel which presents an almost perfect scale free response at high frequency.

摘要

我们展示了一种用于确定粘弹性材料流变学特性的灵活装置,该装置基于沉积在材料平板表面并通过电磁激发的磁体的机械响应。对磁体位移进行干涉测量可在很宽的频率范围内实现极高的精度。除磁体外,被研究材料与仪器之间无接触。在低频时,惯性效应可忽略不计,因此通过锁相放大器获得的机械响应可直接给出材料的复模量。在高频时,会发射阻尼波,流变学特性必须从理论模型中通过数值方法提取。为验证该设计,该仪器被用于测量一种测试聚二甲基硅氧烷凝胶的流变学特性,该凝胶在高频时呈现出几乎完美的无标度响应。

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