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用于保鲜采后白蘑菇的纳米二氧化硅薄膜的合成与表征

Synthesis and Characterization of //Nano-silica Films for the Preservation of Postharvest White Mushrooms.

作者信息

Zhang Rongfei, Wang Xiangyou, Wang Juan, Cheng Meng

机构信息

Department of Food Science and Engineering, Shandong University of Technology, Zibo 255000, China.

出版信息

Polymers (Basel). 2018 Dec 21;11(1):6. doi: 10.3390/polym11010006.

Abstract

In this study, the (KGM)/ (KC)/nano-silica film was prepared and characterized by scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FTIR), and X-ray diffraction (XRD). The preservation quality of white mushrooms () packed using the films was also determined. The nano-silica dosage was found to affect the properties of the nanocomposite KGM/KC films. The results indicated that the properties of the films were significantly improved with the addition of nano-silica. The water vapor permeability, water solubility, moisture absorption, and light transmittance of KGM/KC/nano-silica films were significantly affected by the nano-silica dosage. In this study, the optimal nano-silica dosage to incorporate into the film in order to achieve excellent performance was 0.3%. Strong intermolecular hydrogen bonds were also observed between KGM/KC and nano-silica in the KGM/KC/nano-silica film by FTIR. In addition, the KGM/KC/nano-silica film markedly reduced the browning index, delayed the weight loss and softening, and extended the shelf life of mushrooms during storage at 4 °C. The KGM/KC film modified using nano-silica can provide a potential method for improving the preservation quality of white mushrooms during storage.

摘要

在本研究中,制备了(魔芋葡甘聚糖)/(壳聚糖)/纳米二氧化硅薄膜,并通过扫描电子显微镜(SEM)、傅里叶变换红外光谱(FTIR)和X射线衍射(XRD)对其进行了表征。还测定了使用这些薄膜包装的双孢蘑菇(白蘑菇)的保鲜质量。发现纳米二氧化硅用量会影响纳米复合魔芋葡甘聚糖/壳聚糖薄膜的性能。结果表明,添加纳米二氧化硅后薄膜性能得到显著改善。魔芋葡甘聚糖/壳聚糖/纳米二氧化硅薄膜的水蒸气透过率、水溶性、吸湿性和透光率受纳米二氧化硅用量的显著影响。在本研究中,为实现优异性能而加入到薄膜中的最佳纳米二氧化硅用量为0.3%。通过FTIR还观察到魔芋葡甘聚糖/壳聚糖/纳米二氧化硅薄膜中魔芋葡甘聚糖/壳聚糖与纳米二氧化硅之间存在强分子间氢键。此外,魔芋葡甘聚糖/壳聚糖/纳米二氧化硅薄膜显著降低了褐变指数,延缓了重量损失和软化,并延长了蘑菇在4℃储存期间的货架期。用纳米二氧化硅改性的魔芋葡甘聚糖/壳聚糖薄膜可为提高白蘑菇储存期间的保鲜质量提供一种潜在方法。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3647/6402238/517ca996f437/polymers-11-00006-g001.jpg

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