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自由膜小角中子散射：一种新型的无容器样品环境，可将氢/氘交换降至最低。

Free-film small-angle neutron scattering: a novel container-free sample environment with minimized H/D exchange.

作者信息

Krauss Sebastian W, Schweins Ralf, Magerl Andreas, Zobel Mirijam

机构信息

Chemistry Department, University of Bayreuth, Universitaetsstrasse 30, 95447 Bayreuth, Germany.

Institut Laue-Langevin, DS/LSS, 71 Avenue des Martyrs, Grenoble 38000, France.

出版信息

J Appl Crystallogr. 2019 Feb 26;52(Pt 2):284-288. doi: 10.1107/S1600576719000906. eCollection 2019 Apr 1.

DOI:10.1107/S1600576719000906
PMID:30996715
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC6448684/
Abstract

The development of a container-free sample environment which is particularly well suited for reaction studies of liquid samples by small-angle neutron scattering and related techniques is reported. Hydrogen exchange with the humidity from air is reduced by an encapsulating setup in a bag filled with an inert gas such as He. The effectiveness of this measure is quantitatively accessed by infrared absorption and gravimetry, and further correlated with neutron scattering.

摘要

报道了一种无容器样品环境的开发，该环境特别适合通过小角中子散射及相关技术对液体样品进行反应研究。通过将样品封装在充满惰性气体（如氦气）的袋子中，减少了与空气中湿度的氢交换。通过红外吸收和重量分析法对该措施的有效性进行了定量评估，并进一步与中子散射相关联。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/1be657ef292e/j-52-00284-fig6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/357fe7c13a30/j-52-00284-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/d82b09d266c0/j-52-00284-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/8055fb8249bf/j-52-00284-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/66a6cf128250/j-52-00284-fig4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/bda81ecab4da/j-52-00284-fig5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/1be657ef292e/j-52-00284-fig6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/357fe7c13a30/j-52-00284-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/d82b09d266c0/j-52-00284-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/8055fb8249bf/j-52-00284-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/66a6cf128250/j-52-00284-fig4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/bda81ecab4da/j-52-00284-fig5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fd12/6448684/1be657ef292e/j-52-00284-fig6.jpg

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2
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Biochim Biophys Acta Gen Subj. 2017 Jan;1861(1 Pt B):3693-3699. doi: 10.1016/j.bbagen.2016.04.026. Epub 2016 May 4.
3
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Langmuir. 2015 Sep 22;31(37):10130-6. doi: 10.1021/acs.langmuir.5b02198. Epub 2015 Sep 10.
4
In situ investigation of two-step nucleation and growth of CdS nanoparticles from solution.溶液中CdS纳米颗粒两步成核与生长的原位研究。
Nanoscale. 2015 Jul 14;7(26):11328-33. doi: 10.1039/c5nr01602a.
5
Universal solvent restructuring induced by colloidal nanoparticles.胶态纳米粒子诱导的通用溶剂重组。
Science. 2015 Jan 16;347(6219):292-4. doi: 10.1126/science.1261412.
6
Surfactant-controlled polymerization of semiconductor clusters to quantum dots through competing step-growth and living chain-growth mechanisms.通过竞争的逐步增长和活性链增长机制，控制半导体团簇的表面活性剂聚合为量子点。
J Am Chem Soc. 2012 Oct 17;134(41):17298-305. doi: 10.1021/ja3079576. Epub 2012 Oct 9.
7
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9
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Phys Rev A Gen Phys. 1988 Apr 1;37(7):2580-2589. doi: 10.1103/physreva.37.2580.