Nabeshi Hiromi, Tsutsumi Tomoaki, Matsuda Rieko, Hachisuka Akiko, Akiyama Hiroshi
National Institute of Health Sciences.
Shokuhin Eiseigaku Zasshi. 2019;60(2):7-15. doi: 10.3358/shokueishi.60.7.
To ensure food safety during emergency events such as nuclear disasters, we developed a practical rapid determination method for strontium-90 (Sr-90) in foods. Purification of Sr from foods was simplified using a commercial Sr-extraction column. We also reduced the waiting time to achieve radiative equilibrium between Sr-90 and Y-90. Finally, we developed a rapid determination method for Sr-90 that can be completed in about a week. Using the new method, stable Sr recoveries exceeded 85%. The trueness of the method ranged from 109 to 115% and the detection limit of Sr-90 was estimated to be 0.07 Bq/kg fresh weight according to a performance evaluation using standard materials. Sr-90 radioactivity concentrations in food samples determined by the new method were highly correlated and nearly equal to concentrations determined by the conventional method. The present study suggests that the new method offers highly sensitive and rapid detection of Sr-90 which are necessary attributes for food tests during emergency events.
为确保在核灾难等紧急事件期间的食品安全,我们开发了一种实用的食品中锶-90(Sr-90)快速测定方法。使用商用Sr萃取柱简化了从食品中纯化Sr的过程。我们还缩短了达到Sr-90和Y-90之间辐射平衡的等待时间。最后,我们开发了一种可在约一周内完成的Sr-90快速测定方法。使用新方法,稳定的Sr回收率超过85%。根据使用标准物质的性能评估,该方法的准确性在109%至115%之间,Sr-90的检测限估计为0.07 Bq/kg鲜重。用新方法测定的食品样品中Sr-90放射性浓度与传统方法测定的浓度高度相关且几乎相等。本研究表明,新方法提供了对Sr-90的高灵敏度和快速检测,这是紧急事件期间食品检测的必要属性。