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一种用于水中农药定量分析的改进提取方法。

An improved extraction method for the quantitative analysis of pesticides in water.

作者信息

Brodesser J, Schöler H F

机构信息

Hygiene-Institute University of Bonn.

出版信息

Zentralbl Bakteriol Mikrobiol Hyg B Umwelthyg Krankenhaushyg Arbeitshyg Prav Med. 1987 Oct;185(1-2):183-5.

PMID:3124381
Abstract

An improved method for enrichment and analysis of chloropesticides (5), triazines (1, 4, 6), phosphoric acid esters and other compounds by a rotation perforator according to Ludwig (2, 3) is presented. Water fortified with pesticides was analysed according to this procedure. The organic extract was quantified by gas chromatography. The recovery rates ranged from 80% to more than 110%, whereas those compounds sensitive to hydrolysis and oxidation were insufficient. The above described method was applied to surface water and groundwater analysis.

摘要

介绍了一种根据路德维希(2,3)的方法改进的旋转穿孔器富集和分析氯代农药(5)、三嗪(1,4,6)、磷酸酯及其他化合物的方法。按照该程序对添加了农药的水进行了分析。有机提取物通过气相色谱法定量。回收率在80%至110%以上,但对水解和氧化敏感的那些化合物回收率不足。上述方法应用于地表水和地下水分析。

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