Department of Restorative Dentistry, Faculty of Dentistry.
Department of Metallurgical and Materials Engineering, School of Engineering, Universidade Federal de Minas Gerais (UFMG), Belo Horizonte, Minas Gerais, Brazil.
Int Endod J. 2019 Dec;52(12):1768-1772. doi: 10.1111/iej.13185. Epub 2019 Aug 5.
To compare the martensitic transformation temperatures and torsional resistance behaviour of classic M-Wire Reciproc and Reciproc blue files (VDW, Munich, Germany).
M-Wire classic Reciproc R25 and Reciproc blue R25 instruments were used. Transformation temperatures were determined by differential scanning calorimetry (DSC-DSC 60, Shimadzu, Kyoto, Japan). Three samples with approximately 20 mg of each system were cooled to -120 °C and then heated to 100 °C and then cooled to -100 °C at a rate of 10 °C min . The maximum torque values and angular deflection until fracture of new instruments (n = 10) were measured according to ISO 3630-1. Results were analysed statistically using the Student's t-test at a significance level of P < 0.05.
DSC results revealed the absence of martensitic transformation for Reciproc instruments in the temperature range analysed. In both systems, the instruments were composed of a mixture of R-phase and austenite at room temperature. After torsional tests, Reciproc blue had significantly lower values for mean maximum torque at rupture (P < 0.05), although the angular deflection values were significantly higher than the Reciproc classic group (P < 0.05).
Both Reciproc and Reciproc blue instruments were composed of a mixture of R-phase and austenite. Reciproc Blue instruments had a greater angle of rotation to fracture but a lower torque to failure than M-Wire Reciproc instruments.
比较经典 M-Wire Reciproc 和 Reciproc blue 锉的马氏体相变温度和扭转阻力性能(VDW,慕尼黑,德国)。
使用 M-Wire classic Reciproc R25 和 Reciproc blue R25 器械。通过差示扫描量热法(DSC-DSC 60,岛津,京都,日本)测定相变温度。每个系统取约 20mg 的三个样品,冷却至-120°C,然后以 10°C/min 的速率加热至 100°C,然后再冷却至-100°C。根据 ISO 3630-1 测定新器械(n=10)的最大扭矩值和断裂前的角位移。使用学生 t 检验对结果进行统计学分析,显著水平 P<0.05。
DSC 结果表明,在分析的温度范围内,Reciproc 器械没有马氏体相变。在这两个系统中,器械在室温下由 R 相和奥氏体的混合物组成。扭转试验后,Reciproc blue 的平均最大扭矩断裂值显著降低(P<0.05),尽管角位移值明显高于 Reciproc classic 组(P<0.05)。
Reciproc 和 Reciproc blue 器械均由 R 相和奥氏体的混合物组成。Reciproc Blue 器械的断裂旋转角度更大,但断裂扭矩比 M-Wire Reciproc 器械小。