Tomaselli Lucas de Oliveira, Oliveira Dayane Carvalho Ramos Salles de, Favarão Jamille, Silva Ariel Farias da, Pires-de-Souza Fernanda de Carvalho Panzeri, Geraldeli Saulo, Sinhoreti Mário Alexandre Coelho
Department of Restorative Dentistry, Dental Materials Division, UNICAMP - Universidade de Campinas, Piracicaba, SP, Brazil.
Department of Dentistry, Health and Biological Science Center, UFMT - Universidade Federal de Mato Grosso, Campo Grande, MS, Brazil.
Braz Dent J. 2019 Oct 7;30(5):459-466. doi: 10.1590/0103-6440201902513. eCollection 2019.
The aim of this study was to evaluate of pre-heating, filler contents and ceramic thickness on film thickness, microshear bond strength, degree of conversion and color change on ceramic veneers. Two experimental composites were prepared (Bis-GMA/UDMA/BisEMA/ TEGDMA), with different amounts of filler (65% or 50%wt) simulating a conventional and a flowable composite. The flowable (F) was used at room temperature and, the conventional either at room temperature (C) or pre-heated (CPH). Disk-shaped ceramics with different thickness (0.4 mm, 0.8 mm, 1.5 mm) were prepared. The film thickness was evaluated according to the ISO 4049 (n=10). The microshear bond strength (n=10) was evaluated in enamel using tubing specimens light-cured through the ceramic veneer. The degree of conversion was evaluated using Raman spectroscopy. The color change of the ceramic restorations (n=10) was evaluated by spectrophotometry. The results were submitted to 2-way ANOVA and Tukey's post hoc test (a=5%). For the film thickness 1-way ANOVA was used (a=5%). The C presented the thicker film thickness; the CPH produced a similar film thickness in comparison to the F. All composites showed similar microshear bond strength. The degree of conversion of the F was higher than the C and CPH. The degree of conversion of the composites photo-activated through a 0.4 mm was higher than the composites photo-activated through thicker ceramics. The C showed the highest color change, while the CPH showed similar color change to the F. In conclusion, pre-heated conventional composites seem to be a potential alternative to lute ceramic veneers such as the flowable composites.
本研究的目的是评估预热、填料含量和陶瓷厚度对陶瓷贴面的膜厚度、微剪切粘结强度、转化率和颜色变化的影响。制备了两种实验性复合材料(双酚A-甲基丙烯酸缩水甘油酯/二甲基丙烯酸脲烷/双甲基丙烯酸乙氧基乙酯/三乙二醇二甲基丙烯酸酯),其填料含量不同(65%或50%重量),分别模拟传统复合材料和可流动复合材料。可流动复合材料(F)在室温下使用,传统复合材料在室温下(C)或预热后(CPH)使用。制备了不同厚度(0.4mm、0.8mm、1.5mm)的圆盘状陶瓷。根据ISO 4049评估膜厚度(n=10)。使用通过陶瓷贴面光固化的管状试样在牙釉质中评估微剪切粘结强度(n=10)。使用拉曼光谱法评估转化率。通过分光光度法评估陶瓷修复体的颜色变化(n=10)。结果进行双向方差分析和Tukey事后检验(α=5%)。对于膜厚度,使用单向方差分析(α=5%)。C组的膜厚度最厚;与F组相比,CPH组产生的膜厚度相似。所有复合材料的微剪切粘结强度相似。F组的转化率高于C组和CPH组。通过0.4mm厚陶瓷光活化的复合材料的转化率高于通过较厚陶瓷光活化的复合材料。C组的颜色变化最大,而CPH组的颜色变化与F组相似。总之,预热的传统复合材料似乎是一种潜在的替代材料,可用于粘结陶瓷贴面,如可流动复合材料。