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用于纤维素纸张非接触式谐振腔介电谱研究的方法开发

Method Development for Contactless Resonant Cavity Dielectric Spectroscopic Studies of Cellulosic Paper.

作者信息

Kombolias Mary, Obrzut Jan, Postek Michael T, Poster Dianne L, Obeng Yaw S

机构信息

Testing and Technical Services, Plant Operations, United States Government Publishing Office;

Materials Measurement Laboratory, National Institute of Standards and Technology.

出版信息

J Vis Exp. 2019 Oct 4(152). doi: 10.3791/59991.

Abstract

The current analytical techniques for characterizing printing and graphic arts substrates are largely ex situ and destructive. This limits the amount of data that can be obtained from an individual sample and renders it difficult to produce statistically relevant data for unique and rare materials. Resonant cavity dielectric spectroscopy is a non-destructive, contactless technique which can simultaneously interrogate both sides of a sheeted material and provide measurements which are suitable for statistical interpretations. This offers analysts the ability to quickly discriminate between sheeted materials based on composition and storage history. In this methodology article, we demonstrate how contactless resonant cavity dielectric spectroscopy may be used to differentiate between paper analytes of varying fiber species compositions, to determine the relative age of the paper, and to detect and quantify the amount of post-consumer waste (PCW) recycled fiber content in manufactured office paper.

摘要

目前用于表征印刷和图形艺术基材的分析技术大多是异位且具有破坏性的。这限制了从单个样品中可获得的数据量,并且难以针对独特和稀有材料生成具有统计相关性的数据。谐振腔介电谱是一种非破坏性、非接触式技术,它可以同时检测片状材料的两面,并提供适合进行统计解释的测量结果。这使分析人员能够基于成分和储存历史快速区分片状材料。在这篇方法学文章中,我们展示了如何使用非接触式谐振腔介电谱来区分不同纤维种类组成的纸张分析物、确定纸张的相对年代,以及检测和量化制成办公用纸中消费后废纸(PCW)回收纤维含量。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2a3d/7937941/9e7c44881795/nihms-1548465-f0001.jpg

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