Institute of Nano Science and Nano Technology, University of Kashan, P.O. Box 87317-51167, Kashan, Islamic Republic of Iran.
Chemistry Department, College of Science, University of Raparin, Rania, Kurdistan Region, Iraq.
Ultrason Sonochem. 2020 Mar;61:104840. doi: 10.1016/j.ultsonch.2019.104840. Epub 2019 Oct 24.
Nanoscale cadmium stannate (CdSnO) structures were productively synthesized via a facile and rapid sonochemical route using an eco-friendly capping agent of glucose. In order to optimize the size and structure of products, the various effective factors were inquired such as ultrasound waves, calcination temperature and solvent. The all samples were synthesized under ultrasonic probe for 30 min and different power (frequency) of 80 (24 KHz), 60 (18 KHz) and 40 W (12 KHz). The properties and characteristics of as-fabricated samples were examined by proficient techniques to identification the purity, structure, shape, optical, electrical and surface features. The ability of CdSnO nanostructures and representative graphene based nanocomposites as potential hydrogen storage materials was considered by electrochemical methods. According to the obtained results, the CdSnO/graphene nanocomposites demonstrated higher hydrogen storage capacity than pristine CdSnO nanostructures.
纳米级的锡酸镉（CdSnO）结构通过一种简便、快速的超声化学途径，使用环保的葡萄糖作为封端剂成功合成。为了优化产物的尺寸和结构，研究了各种有效因素，如超声波、煅烧温度和溶剂。所有样品都在超声探头中合成 30 分钟，并采用不同的功率（频率），分别为 80（24 KHz）、60（18 KHz）和 40 W（12 KHz）。通过一系列先进技术对制备的样品进行了性能和特性的检测，以鉴定其纯度、结构、形状、光学、电学和表面特征。通过电化学方法评估了 CdSnO 纳米结构和代表性的基于石墨烯的纳米复合材料作为潜在储氢材料的能力。根据所得结果，CdSnO/石墨烯纳米复合材料比原始的 CdSnO 纳米结构表现出更高的储氢能力。
