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采用三种不同定量评估技术对氧化锆种植体假体进行老化评估。

Ageing assessment of zirconia implant prostheses by three different quantitative assessment techniques.

作者信息

Kyaw Phyu Phyu, Pongprueksa Pong, Anuchitolarn Warangkana, Sirinukunwatta Krongkarn, Suputtamongkol Kallaya

机构信息

Faculty of Dentistry, Mahidol University, Rachathevi, Bangkok, Thailand.

Chemical and Biological Analysis Section, Technical Support for Material Analysis Division, National Metal and Materials Technology Center, Pathum Thani, Thailand.

出版信息

J Adv Prosthodont. 2019 Oct;11(5):253-261. doi: 10.4047/jap.2019.11.5.253. Epub 2019 Oct 30.

DOI:10.4047/jap.2019.11.5.253
PMID:31754415
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC6856306/
Abstract

PURPOSE

To evaluate the influence of cyclic loading on phase transformation of zirconia abutments and to compare the effectiveness of three different quantitative ageing assessment techniques.

MATERIALS AND METHODS

Thirty two Y-TZP prostheses fabricated from two brands, InCoris ZI and Ceramill ZI, were cemented to titanium bases and equally divided into two subgroups (n=8): control group without any treatment and aged group with cyclic loading between 20 N and 98 N for 100,000 cycles at 4 Hz in distilled water at 37℃. The tetragonal-to-monoclinic phase transformation was assessed by (i) conventional x-ray diffraction (XRD), (ii) micro x-ray diffraction (µXRD), and (iii) micro-Raman spectroscopy. The monoclinic-phase fractions (M%) were compared by two-way ANOVA.

RESULTS

InCoris Zi presented significantly higher M% than Ceramill Zi in both control and aged groups (<.001). Both materials exhibited significant phase transformation with monoclinicphase of 1 to 3% more in aged groups than controls for all thre e assessment techniques. The comparable M% was quantified by both µXRD and XRD. The highest M% was assessed with micro-Raman.

CONCLUSION

Cyclic loading produced significant phase transformation in tested Y-TZP prostheses. The micro-Raman spectroscopy could be used as an alternative to XRD and µXRD.

摘要

目的

评估循环加载对氧化锆基台相变的影响,并比较三种不同定量老化评估技术的有效性。

材料与方法

用两种品牌InCoris ZI和Ceramill ZI制作的32个Y-TZP修复体粘结到钛基台上,并平均分为两个亚组(n = 8):未进行任何处理的对照组和在37℃蒸馏水中以4Hz频率在20N至98N之间循环加载100,000次的老化组。通过(i)传统X射线衍射(XRD)、(ii)微X射线衍射(µXRD)和(iii)微拉曼光谱法评估四方相向单斜相的转变。通过双向方差分析比较单斜相分数(M%)。

结果

在对照组和老化组中,InCoris Zi的M%均显著高于Ceramill Zi(<.001)。对于所有三种评估技术,两种材料均表现出显著的相变,老化组的单斜相比对照组多1%至3%。µXRD和XRD对M%的量化结果相当。微拉曼光谱法评估的M%最高。

结论

循环加载在测试的Y-TZP修复体中产生了显著的相变。微拉曼光谱法可作为XRD和µXRD的替代方法。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/238a6f74a00e/jap-11-253-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/9e7b709cfcac/jap-11-253-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/f2274f3d6966/jap-11-253-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/0a474c6b181f/jap-11-253-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/326054770069/jap-11-253-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/fd480d066250/jap-11-253-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/5086db7ccf70/jap-11-253-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/238a6f74a00e/jap-11-253-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/9e7b709cfcac/jap-11-253-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/f2274f3d6966/jap-11-253-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/0a474c6b181f/jap-11-253-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/326054770069/jap-11-253-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/fd480d066250/jap-11-253-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/5086db7ccf70/jap-11-253-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fdd/6856306/238a6f74a00e/jap-11-253-g007.jpg

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本文引用的文献

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2
Effect of hydrothermal degradation on three types of zirconias for dental application.水热降解对三种牙科应用氧化锆的影响。
J Prosthet Dent. 2014 Dec;112(6):1377-84. doi: 10.1016/j.prosdent.2014.07.015. Epub 2014 Sep 30.
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Effects of aging procedures on the topographic surface, structural stability, and mechanical strength of a ZrO2-based dental ceramic.
老化程序对氧化锆基牙科陶瓷的表面形貌、结构稳定性和机械强度的影响。
Dent Mater. 2014 Dec;30(12):e396-404. doi: 10.1016/j.dental.2014.08.380. Epub 2014 Sep 22.
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Eleven-Year Follow-Up of a Prospective Study of Zirconia Implant Abutments Supporting Single All-Ceramic Crowns in Anterior and Premolar Regions.一项关于氧化锆种植体基台支持前牙区和前磨牙区单颗全瓷冠的前瞻性研究的11年随访
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Effect of in vitro aging on the flexural strength and probability to fracture of Y-TZP zirconia ceramics for all-ceramic restorations.体外老化对用于全瓷修复的Y-TZP氧化锆陶瓷弯曲强度和断裂概率的影响。
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Factors affecting the mechanical behavior of Y-TZP.影响钇稳定四方氧化锆多晶体力学行为的因素。
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