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钒对IN718合金激光熔覆组织的影响

Influence of Vanadium on the Microstructure of IN718 Alloy by Laser Cladding.

作者信息

Yang Kun, Xie Hualong, Sun Cong, Zhao Xiaofei, Li Fei

机构信息

Department of Mechanical Engineering and Automation, Northeastern University, Shenyang 110819, China.

Department of Information Science and Engineering, Shenyang University of Technology, Shenyang 110870, China.

出版信息

Materials (Basel). 2019 Nov 21;12(23):3839. doi: 10.3390/ma12233839.

Abstract

A deleterious Laves phase forms in the solidified structure of Inconel 718 (IN718) alloy during laser cladding. However, effective removal methods have not yet been identified. In this study, we first added the IN718 alloy cladding layers with a trace amount of vanadium (V, 0.066 wt.%). Then, we studied the solidification structure of cladding layers using a confocal laser scanning microscope and scanning electron microscopy. The microstructure and Laves phase morphology were investigated. The distribution of niobium (Nb) was observed by experiment as well. We found that V is evenly distributed in dendrites and interdendritic zones. A more refined dendrite structure, reduced second dendrite arm spacing and lower volume fraction of Laves phase were observed in the solidification structure. The results of linear energy-dispersive X-ray spectroscopy (EDS) indicate that the concentration of Nb decreases with an increasing of the distance from the Laves phase. The V-containing sample displayed a relatively slower decreasing tendency. The IN718 alloy sample was harder with the addition of V. In addition, the porosity of the sample decreased compared with the blank sample. The presented findings outline a new method to inhibit the Nb segregation in IN718 alloy during laser cladding, providing reference significance for improving the performance of IN718 alloy samples during actual processing.

摘要

在激光熔覆过程中,Inconel 718(IN718)合金的凝固组织中会形成有害的Laves相。然而,尚未找到有效的去除方法。在本研究中,我们首先向IN718合金熔覆层中添加了微量钒(V,0.066 wt.%)。然后,我们使用共聚焦激光扫描显微镜和扫描电子显微镜研究了熔覆层的凝固组织。对微观结构和Laves相形态进行了研究。还通过实验观察了铌(Nb)的分布。我们发现V均匀分布在枝晶和枝晶间区域。在凝固组织中观察到更细化的枝晶结构、减小的二次枝晶臂间距和更低的Laves相体积分数。能量色散X射线光谱(EDS)分析结果表明,Nb的浓度随着与Laves相距离的增加而降低。含V的样品呈现出相对较慢的下降趋势。添加V后,IN718合金样品硬度增加。此外,与空白样品相比,样品的孔隙率降低。本研究结果概述了一种抑制激光熔覆过程中IN718合金中Nb偏析的新方法,为实际加工过程中提高IN718合金样品的性能提供了参考意义。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/90e1/6926680/3ad802be8de4/materials-12-03839-g001.jpg

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