Department of Prosthodontics, Faculty of Dentistry, Near East University, Lefkosa, Mersin 10, Turkey.
DentX, Lefkosa, Mersin 10, Turkey.
J Esthet Restor Dent. 2020 Jan;32(1):81-90. doi: 10.1111/jerd.12552. Epub 2019 Nov 27.
To investigate the influence of surface treatments conducted in presintering and postsintering stages on flexural strength and optical properties of zirconia.
Specimens were milled from partially sintered zirconia blocks in different geometries and divided into three main groups as presintered, postsintered, and control groups. Test groups were further divided into three subgroups (n = 10) according to the surface treatments conducted (grinding, Er,Cr:YSGG laser irradiation, air-borne particle abrasion [APA]). Four-point flexural strength (σ) test and Weibull analysis were conducted. Color differences (ΔE ) and translucency parameter (TP ) were calculated with a spectrophotometer. Surfaces of specimens were scrutinized under FESEM. Data were statistically analyzed.
Postsintered groups exhibited higher σ values (P < .05). Within all groups, highest and lowest σ values were detected at postsintered and presintered APA groups, respectively (P < .05). All ΔE values were above the perceptibility threshold (ΔE > 0.8). Higher TP values were obtained and deeper scratches were observed in presintered groups.
Surface treatments performed at postsintering stage had a favorable effect on the flexural strength of all specimens. Surface treatments performed before sintering increased translucency and caused higher ΔE values.
Surface treatments performed at different sintering stages can alter mechanical and optical properties of zirconia.
研究预烧和后烧阶段的表面处理对氧化锆弯曲强度和光学性能的影响。
从部分烧结的氧化锆块体中铣削出不同几何形状的试件,并将其分为预烧组、后烧组和对照组三个主要组。试验组根据表面处理(研磨、Er,Cr:YSGG 激光照射、喷丸处理)进一步分为三个亚组(n = 10)。进行四点弯曲强度(σ)测试和威布尔分析。用分光光度计计算颜色差异(ΔE)和透光率参数(TP)。用 FESEM 检查试件表面。对数据进行统计学分析。
后烧组的 σ 值较高(P<.05)。在所有组中,后烧组和预烧组的喷丸处理的 σ 值最高和最低(P<.05)。所有 ΔE 值均超过可察觉阈值(ΔE>0.8)。在预烧组中获得了更高的 TP 值,并且观察到了更深的划痕。
后烧阶段的表面处理对所有试件的弯曲强度均有有利影响。烧结前的表面处理增加了透光率并导致更高的 ΔE 值。
在不同烧结阶段进行的表面处理可以改变氧化锆的机械和光学性能。