Department of Prosthodontics, Faculty of Dentistry, Gazi University.
Department of Chemical Engineering, Faculty of Engineering and Architecture, Gazi University.
Dent Mater J. 2020 Mar 31;39(2):242-250. doi: 10.4012/dmj.2018-259. Epub 2019 Nov 28.
The study aimed to investigate the effects of surface treatments, including plasma, on the peel bond strength between two maxillofacial silicones and two resins with and without thermocycling. Forty-eight experimental groups (n=10) were generated incorporating the two different resins (auto-polymerizing acrylic resin and light-curing urethane dimethacrylate resin [AR and LR, respectively]), two different silicones (M511 and Z004), aging (thermocycled/no thermocycling), and six different surface treatments, including polishing, grinding, polishing+argon plasma, polishing+oxygen plasma, grinding+argon plasma, and grinding+oxygen plasma. Surface topography of a specimen from each surface treatment group was examined by atomic force microscopy. After surface treatments, silicones were polymerized. The peel bond strength values of the control and thermocycled groups were determined. Atomic force microscopy showed that surface topographies of the ground specimens were irregular. Polished specimens showed higher peel bond strength than ground specimens. Plasma application appeared to have improved the bond strength between the resins and silicones.
本研究旨在探讨表面处理(包括等离子体处理)对两种颌面硅橡胶和两种树脂之间的剥离粘结强度的影响,其中包括有和没有热循环处理的情况。通过将两种不同的树脂(自聚合丙烯酸树脂和光固化尿烷二甲基丙烯酸酯树脂[AR 和 LR])、两种不同的硅橡胶(M511 和 Z004)、老化(热循环/无热循环)以及六种不同的表面处理(抛光、研磨、抛光+氩等离子体处理、抛光+氧等离子体处理、研磨+氩等离子体处理和研磨+氧等离子体处理)相结合,共产生了 48 个实验组(n=10)。从每个表面处理组的一个样本中,通过原子力显微镜检查了表面形貌。在进行表面处理后,硅橡胶被聚合。测定了对照组和热循环组的剥离粘结强度值。原子力显微镜显示,研磨后的样本表面形貌不规则。抛光后的样本表现出比研磨后的样本更高的剥离粘结强度。等离子体的应用似乎提高了树脂和硅橡胶之间的粘结强度。