Division of Dental Biomaterials, Tohoku University Graduate School of Dentistry.
Dent Mater J. 2020 Jun 5;39(3):422-428. doi: 10.4012/dmj.2018-394. Epub 2020 Jan 22.
The aim of this study was to construct a Ti-Nb-Cu ternary phase diagram that plays the role of a map for developing new titanium alloys with excellent machinability and mechanical properties. Fifteen experimental Ti-Nb-Cu ternary alloys composed of Ti-5-30%Nb-2-20%Cu were designed, and ingots made using Ar-arc melting furnace before casting to generate specimen. The alloy castings were evaluated in terms of their microstructures and alloy phases. A Ti-Nb-TiCu pseudo-ternary phase diagram was constructed using X-ray diffractmetry results. Three alloy phases (α-Ti, β-Ti and TiCu) were established within the specimen. Furthermore, the prescence of two-phase coexistence regions (α+TiCu, α+β and β+TiCu), and three-phase coexistence region (α+β+TiCu) was noted. The findings obtained through microstructural observation corresponded well with the constructed phase diagram.
本研究旨在构建 Ti-Nb-Cu 三元相图,作为开发具有优异可加工性和机械性能的新型钛合金的指南。设计了 15 种由 Ti-5-30%Nb-2-20%Cu 组成的实验性 Ti-Nb-Cu 三元合金,使用 Ar 电弧熔炼炉进行熔炼以制备铸锭。评估了合金铸锭的微观结构和合金相。利用 X 射线衍射法的结果构建了 Ti-Nb-TiCu 伪三元相图。在试样中确定了三种合金相(α-Ti、β-Ti 和 TiCu)。此外,还观察到了两相共存区(α+TiCu、α+β 和 β+TiCu)和三相共存区(α+β+TiCu)的存在。通过微观结构观察获得的结果与所构建的相图吻合较好。