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结晶度对不同直径浇铸聚酰胺6棒材韧性的影响。

The Effect of Crystallinity on the Toughness of Cast Polyamide 6 Rods with Different Diameters.

作者信息

Odrobina Miklós, Deák Tamás, Székely László, Mankovits Tamás, Keresztes Róbert Zsolt, Kalácska Gábor

机构信息

Institute for Mechanical Engineering Technology, Szent István University, Páter Károly u. 1., H-2100 Gödöllő, Hungary.

R&D Engineer, SimpaTec GmbH; Aspenhaustr. 5, D-72770 Reutlingen, Germany.

出版信息

Polymers (Basel). 2020 Feb 2;12(2):293. doi: 10.3390/polym12020293.

Abstract

The present paper concentrates on the toughness and the degree of crystallinity of the magnesium-catalyzed polyamide 6 rods cast in different diametres, which are commonly used for gear manufacturing. Its toughness cannot be regarded as a constant feature due to the casting technology. The mechanical properties of the semi-finished products are sensitive to the manufactured dimension, e.g., cast diameter, which are investigated by the Charpy impact test and tensile impact test. It is generally accepted that the impact strength and tensile-impact strength correlate with the degree of crystallinity beside many other material's feature. Crystallinity is evaluated by Differential Scanning Calorimetry. The aim of this study is to determine the relationship between toughness and crystallinity of the magnesium-catalyzed cast PA6 rods with different diameters. For the research cast rods between 40 and 300 mm diameter were selected in seven-dimensional steps. Based on the results, it was found that the toughness depends strongly on the diameter size. Furthermore, it is proved that the crystallinity explains 62.3% of the variation of the Charpy's impact strengths, while the tensile impact method was not suitable to detect the difference between the test samples.

摘要

本文着重研究了用于齿轮制造的不同直径的镁催化聚酰胺6铸棒的韧性和结晶度。由于铸造工艺的原因,其韧性不能被视为一个恒定的特性。半成品的机械性能对制造尺寸敏感,例如铸棒直径,通过夏比冲击试验和拉伸冲击试验对其进行研究。除了许多其他材料特性外,冲击强度和拉伸冲击强度通常被认为与结晶度相关。通过差示扫描量热法评估结晶度。本研究的目的是确定不同直径的镁催化铸造聚酰胺6棒的韧性与结晶度之间的关系。为了进行研究,选择了直径在40至300毫米之间、以7毫米为步长的铸棒。基于研究结果发现,韧性强烈依赖于直径尺寸。此外,还证明结晶度解释了夏比冲击强度变化的62.3%,而拉伸冲击法不适用于检测测试样品之间的差异。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eec6/7077395/9e38ab904ef8/polymers-12-00293-g005.jpg

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