Panecatl Bernal Yesmin, Alvarado Joaquin, Rodríguez-Macias Fernando J, Juárez Rodolfo Lima, García-Gallegos Juan Carlos, Chávez-Portillo Melissa, Méndez-Rojas Miguel Ángel
Centro de Investigación en Dispositivos Semiconductores, Instituto de Ciencias, Benemérita Universidad Autónoma de Puebla, Puebla, 2570, México.
Nanotechnology. 2020 Apr 17;31(27):275601. doi: 10.1088/1361-6528/ab7b04. Epub 2020 Feb 28.
We report a method for the efficient anchoring of cadmium selenide (CdSe) nanoparticles on the surface of different types of multi-walled carbon nanotubes (purified, N-doped, O-doped and exfoliated). Characterization using different types of electron microscopies (SEM, STEM, and TEM), energy dispersive spectroscopy (EDS) and x-ray diffraction showed well anchored CdSe nanoparticles (NP) on the nanotube surfaces, NP shapes and sizes varied with temperature and other synthesis conditions, and formed with good yields. The method here reported does not require previous activation of the carbon nanotube surface by chemical functionalization, nor the use of organic solvents, and the reaction proceeded in aqueous solutions, making this process simpler and more environmentally friendly than others.
我们报道了一种将硒化镉(CdSe)纳米颗粒高效锚定在不同类型多壁碳纳米管(纯化的、氮掺杂的、氧掺杂的和剥离的)表面的方法。使用不同类型的电子显微镜(SEM、STEM和TEM)、能量色散光谱(EDS)和X射线衍射进行表征,结果表明CdSe纳米颗粒(NP)很好地锚定在纳米管表面,NP的形状和尺寸随温度及其他合成条件而变化,且产率良好。本文报道的方法不需要预先通过化学功能化对碳纳米管表面进行活化,也不需要使用有机溶剂,反应在水溶液中进行,使得该过程比其他方法更简单、更环保。