异喹啉稠合 N-杂环芳烃的原位空气氧化及光物理研究。
In situ air oxidation and photophysical studies of isoquinoline-fused N-heteroacenes.
机构信息
Department of Chemistry and Biomolecular Science, Faculty of Engineering, Gifu University, Gifu 501-1193, Japan.
出版信息
Org Biomol Chem. 2020 Mar 18;18(11):2129-2138. doi: 10.1039/d0ob00375a.
An efficient, metal free and environment friendly synthesis of isoquinoline-fused benzimidazole has been developed via in situ air oxidation. Also, syntheses of isoquinoline-fused quinazolinone heteroacenes were successfully achieved. The synthesized isoquinoline-fused benzimidazole and isoquinoline-fused quinazolinone derivatives showed λmax, Fmax and Φf values in the ranges 356-394 nm, 403-444 nm and 0.063-0.471, respectively, in CHCl3.
通过原位空气氧化，开发了一种高效、无金属、环保的异喹啉并苯并咪唑的合成方法。此外，还成功地合成了异喹啉并喹唑啉酮杂芳烃。所合成的异喹啉并苯并咪唑和异喹啉并喹唑啉酮衍生物在 CHCl3 中的 λmax、Fmax 和 Φf 值分别在 356-394nm、403-444nm 和 0.063-0.471 范围内。
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