Iqbal Tanveer, Camargo S S, Yasin Saima, Farooq Ujala, Shakeel Ahmad
Department of Chemical, Polymer & Composite Materials Engineering, University of Engineering & Technology, KSK Campus, Lahore 54890, Pakistan.
Department of Materials and Metallurgical Engineering, University Federal do Rio De Janeiro, 21941-901 Rio de Janeiro, Brazil.
Polymers (Basel). 2020 Apr 2;12(4):795. doi: 10.3390/polym12040795.
Nano-indentation, a depth sensing technique, is a useful and exciting tool to investigate the surface mechanical properties of a wide range of materials, particularly polymers. Knowledge of the influence of experimental conditions employed during nano-indentation on the resultant nano-mechanical response is very important for the successful design of engineering components with appropriate surface properties. In this work, nano-indentation experiments were carried out by selecting various values of frequency, amplitude, contact depth, strain rate, holding time, and peak load. The results showed a significant effect of amplitude, frequency, and strain rate on the hardness and modulus of the considered polymer, ultrahigh molecular weight polyethylene (UHMWPE). Load-displacement curves showed a shift towards the lower indentation depths along with an increase in peak load by increasing the indentation amplitude or strain rate. The results also revealed the strong dependence of hardness and modulus on the holding time. The experimental data of creep depth as a function of holding time was successfully fitted with a logarithmic creep model (R ≥ 0.98). In order to remove the creeping effect and the nose problem, recommended holding times were proposed for the investigated polymer as a function of different applied loads.
纳米压痕作为一种深度传感技术,是研究多种材料尤其是聚合物表面力学性能的一种有用且令人兴奋的工具。了解纳米压痕过程中所采用的实验条件对所得纳米力学响应的影响,对于成功设计具有适当表面性能的工程部件非常重要。在这项工作中,通过选择频率、振幅、接触深度、应变速率、保持时间和峰值载荷的各种值进行了纳米压痕实验。结果表明,振幅、频率和应变速率对所研究的聚合物——超高分子量聚乙烯(UHMWPE)的硬度和模量有显著影响。载荷-位移曲线显示,通过增加压痕振幅或应变速率,随着峰值载荷的增加,曲线向较低的压痕深度偏移。结果还揭示了硬度和模量对保持时间的强烈依赖性。蠕变深度作为保持时间函数的实验数据成功地用对数蠕变模型拟合(R≥0.98)。为了消除蠕变效应和“鼻尖”问题,针对所研究的聚合物,根据不同的施加载荷提出了推荐的保持时间。