Minissale M, Durif A, Hiret P, Vidal T, Faucheux J, Lenci M, Mondon M, Kermouche G, Pontillon Y, Grisolia C, Richou M, Gallais L
Aix Marseille Univ, CNRS, PIIM, Marseille, France.
CEA, IRFM, F-13108 Saint-Paul-Lez-Durance, France.
Rev Sci Instrum. 2020 Mar 1;91(3):035102. doi: 10.1063/1.5133741.
The knowledge of material properties and their behavior at high temperatures is of crucial importance in many fields. For instance, annealing phenomena occurring during the thermomechanical processing of materials, such as recrystallization, have long been recognized as being both of scientific interest and technological importance. Different methods are currently used to study annealing phenomena and submit metals to heat loads. In this work, we present the design and the development of a laser-based facility for annealing tests. This experimental setup enables studies at the laboratory scale with great flexibility to submit samples to various spatial and temporal heating profiles. Due to the possibility of having optical access to the sample, laser heating can be combined with several non-contact diagnostics such as infrared imaging to control and analyze the temperature gradients. As a case study, we present a set of experiments performed to study the recrystallization kinetics of tungsten. We demonstrate that samples can be heated linearly with heating rate up to ∼2000 K/s, at temperatures above 2000 K, for seconds or hours, with typical errors in the temperature measurement of around 1% that depend mainly on the determination of sample emissivity. Such studies are of crucial interest in the framework of nuclear fusion since the international thermonuclear experimental reactor nuclear reactor will operate with a full-W divertor.
材料特性及其在高温下的行为知识在许多领域都至关重要。例如,材料热机械加工过程中出现的退火现象,如再结晶,长期以来一直被认为既具有科学研究价值又具有技术重要性。目前采用不同方法来研究退火现象并使金属承受热负荷。在这项工作中,我们展示了一种基于激光的退火测试设备的设计与开发。这种实验装置能够在实验室规模上进行研究,具有很大的灵活性,可使样品承受各种空间和时间加热曲线。由于能够对样品进行光学观察,激光加热可与多种非接触诊断方法相结合,如红外成像,以控制和分析温度梯度。作为一个案例研究,我们展示了一组为研究钨的再结晶动力学而进行的实验。我们证明,样品能够在高于2000 K的温度下以高达约2000 K/s的加热速率线性加热数秒或数小时,温度测量的典型误差约为1%,这主要取决于样品发射率的测定。这类研究在核聚变框架内至关重要,因为国际热核聚变实验反应堆将采用全钨偏滤器运行。