Lewis A J
J Biomed Mater Res. 1977 May;11(3):447-58. doi: 10.1002/jbm.820110311.
A series of tensile test pieces of the dimensions stated in the American Dental Association Specification No. 14 were produce using both nickel-base and cobalt-base removable partial denture casting alloys. Normal dental casting techniques were employed. Appropriate sections from each specimen were sectioned to half of their original thicknesses, embedded in heat-and pressure-cured conducting mounts, and polished for metallurgical examination. A double electrolytic etching technique was used, employing serially two solutions, in order to maximize the amount of metallographic detail visible. The method proved particularly valuable in the case of the nickel-base alloy as it indicated the presence of considerable interdendritic segregation. The incidence of porosity was evaluated throughout all sections of the specimens and, although found to be especially prevalent in those regions where gross shrinkage effects might be expected to occur, it was also shown to have a diffuse intergranular and interdendritic distribution.
使用镍基和钴基可摘局部义齿铸造合金制作了一系列符合美国牙科协会第14号规范所述尺寸的拉伸试件。采用了常规的牙科铸造技术。从每个试样上截取适当的部分,将其厚度减半,嵌入热压固化的导电镶嵌块中,并进行抛光以进行金相检验。采用双电解蚀刻技术,依次使用两种溶液,以最大限度地增加可见的金相细节数量。该方法在镍基合金的情况下特别有价值,因为它表明存在相当多的枝晶间偏析。对试样的所有截面进行了气孔率评估,尽管发现气孔率在预期会出现严重收缩效应的区域特别普遍,但也显示出其具有沿晶界和枝晶间的弥散分布。