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表面涂层和一年的水老化如何影响释氟修复材料的性能?

How do the surface coating and one-year water aging affect the properties of fluoride-releasing restorative materials?

作者信息

Ugurlu M

机构信息

Department of Restorative Dentistry, Faculty of Dentistry, Süleyman Demirel University, Isparta, Turkey.

出版信息

Niger J Clin Pract. 2020 May;23(5):720-728. doi: 10.4103/njcp.njcp_591_19.

DOI:10.4103/njcp.njcp_591_19
PMID:32367882
Abstract

OBJECTIVE

To evaluate the effects of surface coating and 1-year water aging on flexural strength, compressive strength (CS) and surface roughness of fluoride-releasing restorative materials.

MATERIALS AND METHODS

The specimens were prepared from seven materials: GCP Glass Fill (GCP), Amalgomer CR (AHL), Zirconomer (Shofu), Fuji IX GP Capsule (GC), Beautifil II (Shofu), Estelite Σ Quick (Tokuyama), and reliaFIL LC (AHL). The specimens were randomly divided into two groups for each test: surface coated with G-Coat Plus (GC) and uncoated. Each group was subdivided into two groups stored in distilled water at 37°C for 24 h and 1 year before testing (n = 10). The flexural and CS were evaluated according to ISO standards on a universal testing machine. The surface roughness was assessed with AFM. After flexural strength test, a cross-section of the coated specimens was evaluated with SEM. Data were analyzed with one-way analysis of variance, Duncan and independent t-tests (P = 0.05).

RESULTS

After 24 h, a significant increase was observed on the flexural and CS of Amalgomer CR, Zirconomer, and Fuji IX GP by coating (P < 0.05). After 1 year, the coating increased the flexural strength of Amalgomer CR and Zirconomer, and CS of GCP Glass Fill (P < 0.05). The coating decreased the surface roughness of GCP Glass Fill, Amalgomer CR, and Zirconomer after 1 year (P < 0.05). The water aging decreased the mechanical properties of glass ionomer-based materials and increased their surface roughness (P < 0.05).

CONCLUSION

The mechanical properties and surface roughness of glass ionomer-based materials were affected by coating and water aging.

摘要

目的

评估表面涂层和1年水老化对释氟修复材料的弯曲强度、抗压强度(CS)及表面粗糙度的影响。

材料与方法

用七种材料制备标本:GCP玻璃填料(GCP)、Amalgomer CR(AHL)、Zirconomer(松风)、富士IX GP胶囊(GC)、Beautifil II(松风)、Estelite Σ Quick(德山)和reliafil LC(AHL)。每个测试的标本随机分为两组:用G-Coat Plus(GC)表面涂层和未涂层。每组再细分为两组,在测试前分别于37°C蒸馏水中保存24小时和1年(n = 10)。根据ISO标准在万能试验机上评估弯曲强度和抗压强度。用原子力显微镜评估表面粗糙度。弯曲强度测试后,用扫描电子显微镜评估涂层标本的横截面。数据采用单因素方差分析、邓肯检验和独立t检验进行分析(P = 0.05)。

结果

24小时后,涂层使Amalgomer CR、Zirconomer和富士IX GP的弯曲强度和抗压强度显著增加(P < 0.05)。1年后,涂层提高了Amalgomer CR和Zirconomer的弯曲强度以及GCP玻璃填料的抗压强度(P < 0.05)。1年后,涂层降低了GCP玻璃填料、Amalgomer CR和Zirconomer的表面粗糙度(P < 0.05)。水老化降低了玻璃离子体基材料的力学性能并增加了其表面粗糙度(P < 0.05)。

结论

玻璃离子体基材料的力学性能和表面粗糙度受涂层和水老化的影响。

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